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77709-02-5

4,6-DIAMINOPYRIMIDINE HEMISULFATE, MONOHYDRATE, 98

Product Name 4,6-DIAMINOPYRIMIDINE HEMISULFATE, MONOHYDRATE, 98

CAS77709-02-5

MFC4H8N4O4S

MW208.19

  • 77709-02-5_ms_1
    Mass

    MS-NW-7873          
    4,6-pyrimidinediamine hemisulfate
    C4H6N4 1/2H2O4S     (Mass of molecular ion:    110)
    

       Source Temperature: 190 °C
       Sample Temperature: 200 °C
       Direct, 75 eV
    

          17.0       2.7
          18.0      15.0
          27.0       2.1
          28.0      15.8
          29.0       2.4
          38.0       1.0
          39.0       2.8
          40.0      12.6
          41.0      24.9
          42.0       3.9
          43.0      16.1
          44.0       2.1
          45.0       1.6
          53.0       1.6
          54.0       1.2
          55.0      10.1
          56.0       9.1
          65.0       1.0
          66.0       9.0
          67.0      23.0
          68.0       4.4
          70.0       3.0
          82.0       2.5
          83.0      33.1
          84.0       1.4
         110.0     100.0
         111.0       6.3
    

400 MHz in DMSO-d6

  • 77709-02-5_1hnmr_1

    1H NMR 399.65 MHz
    C4 H6 N4 0.038 g : 0.5 ml DMSO-d6
    4,6-pyrimidinediamine hemisulfate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.046 B *1 7.23 C *1 5.9 D 5.543

         Hz     ppm     Int.
    

       3216.19   8.048    949
       2887.45   7.225    277
       2359.38   5.904     59
       2215.94   5.545    891
       2215.21   5.543   1000
    

in DMSO-d6

  • 77709-02-5_13cnmr_1

KBr disc

  • 77709-02-5_ir1_2

nujol mull

  • 77709-02-5_ir2_1