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MassMS-NW-5220 9,10-dihydrophenanthrene C14H12 (Mass of molecular ion: 180)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
28.0 1.4 39.0 2.3 50.0 1.6 51.0 3.0 62.0 1.6 63.0 4.6 74.0 2.0 75.0 3.5 76.0 10.8 76.5 1.7 77.0 2.1 82.5 3.6 87.0 1.7 88.0 6.3 88.5 1.5 89.0 14.7 89.5 3.8 90.0 4.0 115.0 2.4 126.0 1.5 127.0 1.2 128.0 1.9 129.0 1.0 139.0 1.9 141.0 2.2 143.0 1.0 145.0 1.0 150.0 2.5 151.0 5.1 152.0 8.3 153.0 3.0 154.0 3.1 158.0 2.3 163.0 1.1 164.0 1.0 165.0 25.7 166.0 4.2 167.0 1.2 175.0 1.1 176.0 8.3 177.0 6.5 178.0 36.3 179.0 61.2 180.0 100.0 181.0 15.4 182.0 5.9 186.0 3.2
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C14 H12 18.5 mg : 0.5 ml CDCl3 9,10-dihydrophenanthrene 
Assign. Shift(ppm)
A 7.747 B 7.294 C 7.23 D 7.22 E 2.868 CONFIRMED BY LAOCN PROGRAM.
Hz ppm Int.3100.10 7.758 164 3092.29 7.738 176 2924.80 7.319 57 2921.02 7.309 58 2919.68 7.306 91 2917.11 7.300 76 2916.02 7.297 108 2913.57 7.291 59 2911.87 7.287 101 2908.33 7.278 107 2893.07 7.240 38 2889.65 7.231 466 2888.79 7.229 437 2886.11 7.222 279 2884.40 7.218 210 2883.18 7.215 172 2876.95 7.199 35 1146.24 2.869 1000
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1H NMR 89.56 MHz C14 H12 0.04 ml : 0.5 ml CDCl3 9,10-dihydrophenanthrene Assign. Shift(ppm)
A 7.74 B 7.29 C 7.22 D 7.21 E 2.87 400MHZ : HSP-40-237
Hz ppm Int.696.88 7.782 60 695.44 7.766 58 693.69 7.746 110 691.75 7.724 52 688.88 7.692 130 687.19 7.673 121 660.88 7.380 39 656.13 7.327 118 653.94 7.302 36 651.56 7.276 175 649.31 7.251 58 648.56 7.242 89 646.81 7.223 423 645.00 7.202 786 643.94 7.191 181 642.38 7.173 101 641.63 7.165 138 641.00 7.158 123 639.00 7.135 25 254.69 2.844 1000
in CDCl3
liquid film
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