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MassMS-NW-4946 3,4-dichloro-1-butene C4H6Cl2 (Mass of molecular ion: 124)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
26.0 6.6 27.0 27.8 28.0 3.2 35.0 1.0 36.0 3.1 37.0 2.1 38.0 3.1 39.0 35.7 40.0 1.6 41.0 1.1 49.0 9.5 50.0 6.0 51.0 9.8 52.0 3.7 53.0 38.1 54.0 6.1 61.0 3.7 62.0 7.4 63.0 2.4 64.0 2.4 73.0 1.4 75.0 100.0 76.0 3.6 77.0 31.8 78.0 1.1 87.0 1.2 88.0 20.8 89.0 43.7 90.0 8.8 91.0 14.2 124.0 2.0 126.0 1.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C4 H6 Cl2 0.05 ml : 0.5 ml CDCl3 3,4-dichloro-1-butene 
Assign. Shift(ppm)
A 5.887 B 5.430 C 5.325 D 4.495 E *1 3.781 F *1 3.676
Hz ppm Int.2371.09 5.933 347 2363.04 5.913 375 2360.96 5.908 391 2354.25 5.891 444 2352.91 5.888 418 2346.19 5.871 444 2344.12 5.866 457 2336.06 5.846 454 2181.76 5.460 41 2178.83 5.452 592 2177.86 5.450 952 2177.00 5.448 595 2161.87 5.410 513 2161.01 5.408 821 2160.16 5.406 490 2133.79 5.340 620 2133.06 5.338 956 2132.32 5.336 574 2123.66 5.314 562 2122.92 5.312 880 2122.07 5.310 545 1807.62 4.524 146 1806.88 4.522 223 1806.03 4.520 145 1802.12 4.510 169 1801.39 4.508 251 1800.42 4.505 203 1799.68 4.504 286 1798.83 4.502 412 1798.10 4.500 268 1794.19 4.490 278 1793.33 4.488 424 1792.48 4.486 287 1791.75 4.484 198 1790.89 4.482 251 1790.04 4.480 159 1788.09 4.475 31 1786.13 4.470 151 1785.40 4.468 232 1784.55 4.466 149 1520.87 3.806 638 1515.38 3.792 624 1509.64 3.778 1000 1504.15 3.764 950 1477.42 3.697 989 1469.48 3.677 961 1466.19 3.669 643 1458.25 3.649 622
in CDCl3
liquid film
4880 A,200 M,liquid
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