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2,2,2-Tribromoethanol

Product Name 2,2,2-Tribromoethanol

CAS75-80-9

MFC2H3Br3O

MW282.76

¹³CNMR

Mass

MS-IW-4895          
2,2,2-tribromoethanol
C2H3Br3O            (Mass of molecular ion:    280)

   Source Temperature: 230 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      14.0       4.4
      15.0       4.5
      18.0       1.4
      25.0       1.9
      26.0       7.5
      28.0       2.3
      29.0       8.7
      30.0       1.1
      31.0      78.1
      41.0       3.5
      42.0      14.4
      43.0      11.9
      44.0       1.8
      79.0      13.6
      80.0      10.3
      81.0      13.7
      82.0      10.2
      91.0      11.5
      92.0       8.3
      93.0      58.9
      94.0       9.9
      95.0      47.9
      96.0       1.8
     104.0       2.8
     105.0       5.0
     106.0       2.8
     107.0       4.8
     120.0       2.4
     121.0      63.1
     122.0       8.5
     123.0      62.5
     124.0       6.0
     160.0       1.9
     170.0       7.9
     171.0       6.0
     172.0      17.8
     173.0      12.0
     174.0      12.1
     175.0       6.3
     176.0       2.3
     184.0       1.2
     186.0       2.4
     188.0       1.1
     200.0       1.6
     201.0      51.8
     202.0       4.1
     203.0     100.0
     204.0       3.6
     205.0      48.8
     206.0       1.1
     249.0       2.6
     251.0       7.6
     252.0       1.8
     253.0       7.5
     254.0       1.7
     255.0       2.5

400 MHz in CDCl3

90 MHz in CDCl3

¹H NMR	399.65 MHz
C₂ H₃ Br₃ O	0.039 g : 0.5 ml CDCl₃
2,2,2-tribromoethanol

    Assign.     Shift(ppm)

      A             4.283
      B             3.11

     Hz     ppm     Int.

   1715.94   4.294    966
   1712.40   4.285     25
   1708.13   4.275   1000
   1250.12   3.129    254
   1242.31   3.109    503
   1234.38   3.089    238

¹H NMR	89.56 MHz
C₂ H₃ Br₃ O	0.039 g : 0.5 ml CDCl₃
2,2,2-tribromoethanol

    Assign.     Shift(ppm)

      A             4.26
      B             3.1

     Hz     ppm     Int.

    381.81   4.264   1000
    276.31   3.086    259

in CDCl3

KBr disc

nujol mull

4880 A,200 M,powder

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