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MS-NW-1151 propyleneimine C3H7N (Mass of molecular ion: 57)
Source Temperature: 240 °C Sample Temperature: 170 °C Reservoir, 75 eV
14.0 1.3 15.0 8.5 17.0 1.2 18.0 5.4 26.0 7.3 26.5 1.4 27.0 15.5 28.0 100.0 29.0 27.4 30.0 37.3 32.0 1.7 38.0 1.7 39.0 4.9 40.0 4.0 41.0 7.2 42.0 18.0 43.0 1.0 44.0 3.7 51.0 1.2 52.0 2.1 54.0 3.5 55.0 1.3 56.0 82.4 57.0 56.8 58.0 3.3 71.0 1.7
90 MHz in CDCl3
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1H NMR 89.56 MHz C3 H7 N 0.04 ml : 0.5 ml CDCl3 propyleneimine Assign. Shift(ppm)
A 1.98 B *1 1.75 C *1 1.30 D 1.204 E 0.24
Hz ppm Int.
185.89 2.076 75 182.37 2.037 82 180.54 2.016 108 180.18 2.012 105 177.10 1.978 112 176.73 1.974 114 175.34 1.958 81 174.83 1.953 105 171.97 1.921 84 171.31 1.913 111 159.16 1.778 314 153.44 1.714 197 117.63 1.314 316 114.26 1.276 283 110.23 1.231 1000 108.03 1.207 77 104.96 1.172 840 20.73 0.232 82
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