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D-Lysine hydrochloride

Product Name D-Lysine hydrochloride

CAS7274-88-6

MFC6H15ClN2O2

MW182.65

¹³CNMR

Mass

MS-IW-4171          
D-lysine monohydrochloride
C6H14N2O2 HCl       (Mass of molecular ion:    146)

   Source Temperature: 190 °C
   Sample Temperature: 180 °C
   Direct, 75 eV

      15.0       1.1
      17.0       2.1
      18.0      14.2
      27.0       3.9
      28.0      22.3
      29.0       7.2
      30.0      79.0
      31.0       3.1
      35.0       5.2
      36.0      66.1
      37.0       1.8
      38.0      22.2
      39.0       3.3
      41.0      11.4
      42.0      12.9
      43.0      23.0
      44.0      17.1
      45.0       4.7
      46.0       1.9
      53.0       1.5
      54.0       3.9
      55.0      12.8
      56.0      71.0
      57.0      14.8
      58.0       3.5
      59.0       8.4
      65.0       1.1
      67.0      10.0
      68.0       2.1
      69.0       4.8
      70.0       9.7
      71.0      10.9
      72.0      87.6
      73.0       9.4
      74.0      20.1
      75.0       5.2
      81.0       1.0
      82.0       9.5
      83.0      12.2
      84.0     100.0
      85.0       9.2
      87.0       2.6
      88.0       3.1
      89.0       3.0
      99.0       2.2
     100.0      10.0
     101.0       6.3
     110.0       2.1
     111.0       3.3
     112.0       1.6
     117.0       3.7
     128.0       6.0
     129.0      14.0
     130.0       7.2
     146.0       1.0
     147.0       4.4

400 MHz in D2O

¹H NMR	399.65 MHz
C₆ H₁₄ N₂ O₂	0.040 g : 0.5 ml D₂O
D-lysine monohydrochloride

    Assign.     Shift(ppm)

      A             3.766
      B             3.034
      C             1.911
      D             1.732
      E             1.485
     
     SOLVENT PEAK REMOVED

     Hz     ppm     Int.

   1511.60   3.783    375
   1505.37   3.767    727
   1499.39   3.752    389
   1220.46   3.054    764
   1212.89   3.035   1000
   1205.20   3.016    809
    785.03   1.965     40
    777.10   1.945    164
    774.05   1.937    184
    770.87   1.929    284
    767.46   1.921    483
    764.65   1.914    322
    760.86   1.904    448
    757.93   1.897    355
    754.64   1.889    211
    751.59   1.881    197
    743.65   1.861     55
    708.50   1.773    139
    700.56   1.753    417
    692.99   1.734    603
    685.42   1.716    492
    677.98   1.697    211
    628.66   1.574     41
    621.34   1.555     86
    615.48   1.541    104
    614.38   1.538     99
    612.43   1.533    100
    608.15   1.522    172
    606.08   1.517    146
    599.24   1.500    238
    591.55   1.481    240
    583.98   1.462    211
    580.32   1.453    110
    577.15   1.445    135
    571.04   1.429     84
    561.77   1.406     53

in D2O

KBr disc

nujol mull

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