-
MassMS-NW-2389 1,1-dichloro-2,2-bis(p-chlorophenyl)ethane C14H10Cl4 (Mass of molecular ion: 318)
Source Temperature: 180 °C Sample Temperature: 120 °C Direct, 75 eV
17.0 1.3 18.0 6.8 28.0 1.5 36.0 2.3 39.0 1.2 50.0 3.4 51.0 3.4 62.0 1.2 63.0 2.4 73.0 1.3 74.0 2.8 75.0 6.9 76.0 1.9 77.0 1.1 81.5 1.4 82.0 4.4 82.5 1.8 85.0 1.0 87.0 1.6 88.0 4.9 88.5 1.2 89.0 1.5 93.0 1.0 99.0 2.1 99.5 2.0 100.0 2.0 101.0 4.1 102.0 2.3 106.0 2.4 111.0 1.3 123.0 1.0 136.0 3.4 137.0 3.4 138.0 1.6 139.0 1.6 150.0 1.0 151.0 1.6 163.0 3.6 164.0 4.1 165.0 39.0 166.0 5.7 172.0 1.6 173.0 1.0 174.0 1.4 175.0 1.3 176.0 6.1 177.0 3.0 178.0 6.2 179.0 1.0 199.0 11.1 200.0 6.4 201.0 4.8 202.0 2.2 212.0 7.3 213.0 1.8 214.0 2.4 235.0 100.0 236.0 14.3 237.0 63.5 238.0 9.0 239.0 10.4 240.0 1.4 246.0 1.0 247.0 1.2 248.0 2.5 249.0 1.1 250.0 1.3 282.0 1.1 284.0 1.0 318.0 2.1 320.0 2.8 322.0 1.3
90 MHz in CDCl3
-
1H NMR 89.56 MHz C14 H10 Cl4 0.045 g : 0.5 ml CDCl3 1,1-dichloro-2,2-bis(p-chlorophenyl)ethane 
Assign. Shift(ppm)
A 7.29 B 7.25 C 6.285 D 4.54
Hz ppm Int.660.94 7.380 53 660.56 7.376 52 659.81 7.368 53 657.50 7.342 41 654.81 7.312 50 651.75 7.278 1000 650.88 7.268 712 650.25 7.261 937 648.44 7.241 166 647.00 7.225 66 644.63 7.198 35 641.81 7.167 39 641.13 7.159 49 567.06 6.332 231 559.06 6.243 258 410.63 4.585 118 402.69 4.497 107
in CDCl3
CCl4 solution
KBr disc
nujol mull
4880 A,100M,powder
More Suppliers
