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1-(2-Aminoethyl)pyrrolidine

Product Name 1-(2-Aminoethyl)pyrrolidine

CAS7154-73-6

MFC6H14N2

MW114.19

¹³CNMR

Mass

MS-NW-1220          
1-(2-aminoethyl)pyrrolidine
C6H14N2             (Mass of molecular ion:    114)

   Source Temperature: 250 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       2.7
      18.0       2.7
      27.0       3.5
      28.0       6.8
      29.0       3.0
      30.0      10.3
      39.0       2.0
      41.0       4.2
      42.0      29.8
      43.0       4.6
      44.0       4.1
      54.0       1.3
      55.0      13.7
      56.0       4.4
      57.0       1.4
      70.0       3.9
      82.0       1.1
      84.0     100.0
      85.0       6.3
     114.0       3.2

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₆ H₁₄ N₂	0.04 ml : 0.5 ml CDCl₃
1-(2-aminoethyl)pyrrolidine

    Assign.     Shift(ppm)

      A             2.807
      B             2.53
      C             2.51
      D             1.77
      E             1.61

     Hz     ppm     Int.

    260.13   2.905    218
    258.38   2.885    253
    254.50   2.842    295
    252.94   2.825    382
    252.19   2.816    895
    247.31   2.762    580
    246.25   2.750    665
    236.06   2.636     39
    234.69   2.621     47
    232.69   2.599    660
    231.69   2.587    673
    230.63   2.576    260
    230.00   2.569    254
    229.19   2.560    211
    228.19   2.548    256
    227.75   2.543    273
    226.81   2.533   1000
    226.13   2.525    659
    225.06   2.513    725
    224.56   2.508    685
    223.44   2.495    404
    222.88   2.489    481
    221.81   2.477    250
    220.69   2.465    425
    219.50   2.451    370
    218.63   2.442    460
    215.69   2.409     66
    214.75   2.398     73
    214.13   2.391     59
    173.06   1.933     45
    172.13   1.922     37
    168.13   1.878     70
    165.00   1.843    320
    163.25   1.823    214
    162.06   1.810    366
    161.06   1.799    297
    159.88   1.786    303
    159.38   1.780    321
    158.38   1.769    878
    156.56   1.749    260
    154.63   1.727    387
    153.44   1.714    155
    151.88   1.696    220
    151.50   1.692    220
    148.75   1.661    199
    147.56   1.648    210
    144.25   1.611    281
    142.31   1.589    254

in CDCl3

CCl4 solution

liquid film

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