3-METHYLTHIOPROPIONYL CHLORIDE

Mass

MS-IW-9175          
3-(methylthio)propionyl chloride
C4H7ClOS            (Mass of molecular ion:    138)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       2.1
      25.0       1.4
      26.0       8.4
      27.0      46.6
      28.0       9.2
      29.0       1.7
      32.0       1.3
      35.0       8.8
      36.0      11.8
      37.0       1.2
      38.0       4.1
      39.0       1.4
      41.0      10.9
      42.0       1.5
      44.0       2.2
      45.0      23.2
      46.0      11.0
      47.0      25.0
      48.0       8.1
      49.0       5.6
      51.5       1.2
      53.0       1.5
      54.0       1.2
      55.0     100.0
      56.0       4.4
      57.0       2.8
      58.0       6.1
      59.0      11.1
      60.0       2.7
      61.0      55.0
      62.0       2.1
      63.0       7.1
      65.0       1.6
      73.0       1.5
      74.0      11.7
      75.0      32.3
      76.0       2.1
      77.0       1.5
      82.0       1.6
      91.0       2.0
      95.0       1.6
     101.0       1.0
     102.0      33.8
     103.0       8.3
     104.0       2.0
     138.0      22.8
     139.0       1.2
     140.0       8.3
     150.0       1.6

Assign. Shift(ppm) A 3.210 B 2.817 C 2.155

     Hz     ppm     Int.

   1289.92   3.228    556
   1286.25   3.219     59
   1282.84   3.210   1000
   1278.69   3.200     53
   1275.63   3.192    641
   1133.06   2.836    138
   1126.22   2.819    205
   1119.51   2.802    117
    861.21   2.155    521