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MS-NW-7333 (-)-alpha-ethylphenethyl alcohol C10H14O (Mass of molecular ion: 150)
Source Temperature: 210 °C Sample Temperature: 190 °C Reservoir, 75 eV
27.0 1.6 29.0 1.9 31.0 7.9 39.0 3.4 41.0 4.9 43.0 1.0 50.0 1.0 51.0 3.1 57.0 2.0 59.0 19.5 63.0 1.9 65.0 6.7 77.0 4.0 78.0 1.4 79.0 1.4 89.0 1.5 91.0 40.8 92.0 100.0 93.0 8.5 103.0 5.8 121.0 5.9
90 MHz in CDCl3
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1H NMR 89.56 MHz C10 H14 O 0.05 ml : 0.5 ml CDCl3 (-)-alpha-ethylphenethyl alcohol Assign. Shift(ppm)
A 7.23 to 7.21 B 3.693 C *1 2.77 D *1 2.62 E 1.92 F 1.49 G 0.97 J(B,C)=4.7HZ J(B,D)=8.0HZ
Hz ppm Int.
663.00 7.403 32 659.69 7.366 43 657.00 7.336 63 654.69 7.311 76 651.88 7.279 193 651.13 7.271 183 650.19 7.260 189 647.63 7.232 1000 646.19 7.216 903 643.38 7.184 227 641.38 7.162 144 640.75 7.155 148 638.56 7.130 103 635.63 7.098 44 633.75 7.077 38 632.81 7.066 34 338.13 3.776 55 336.94 3.763 49 336.75 3.761 49 335.44 3.746 50 332.81 3.717 55 330.69 3.693 78 328.94 3.673 57 326.31 3.644 51 325.31 3.633 57 325.00 3.629 57 323.94 3.618 66 318.63 3.558 35 260.75 2.912 38 255.88 2.858 46 247.19 2.761 226 242.44 2.708 427 238.31 2.661 36 237.81 2.656 35 237.38 2.651 36 236.88 2.645 37 234.56 2.620 204 228.94 2.557 51 221.13 2.470 49 171.75 1.918 206 150.38 1.680 38 148.31 1.656 38 148.06 1.654 38 145.00 1.620 42 143.88 1.607 56 142.00 1.586 134 140.94 1.574 111 138.69 1.549 57 136.50 1.525 129 134.13 1.498 281 131.25 1.466 69 128.63 1.437 166 127.31 1.422 195 124.06 1.386 32 123.75 1.382 32 121.38 1.356 106 112.88 1.261 32 93.06 1.040 374 86.31 0.964 634 78.56 0.878 199 77.13 0.862 123