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MassMS-NW-9669 o-methoxyphenyl isocyanate C8H7NO2 (Mass of molecular ion: 149)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
26.0 1.1 27.0 3.1 28.0 2.5 37.0 1.3 38.0 2.1 39.0 3.5 50.0 3.5 51.0 17.1 52.0 5.0 62.0 1.0 63.0 2.9 64.0 2.5 65.0 1.6 66.0 1.3 76.0 1.5 77.0 2.2 78.0 25.1 79.0 2.8 90.0 2.1 92.0 1.3 93.0 3.5 106.0 37.4 107.0 2.7 108.0 4.5 120.0 44.5 121.0 4.4 134.0 51.3 135.0 4.3 148.0 1.2 149.0 100.0 150.0 9.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H7 N O2 0.05 ml : 0.5 ml CDCl3 o-methoxyphenyl isocyanate 
Assign. Shift(ppm)
A 7.104 B 6.948 C 6.84 D 6.83 E 3.857
Hz ppm Int.2848.27 7.127 89 2846.56 7.123 94 2840.70 7.108 147 2840.09 7.107 127 2838.62 7.103 181 2832.52 7.088 114 2830.81 7.084 123 2782.23 6.962 113 2781.49 6.960 95 2780.52 6.958 147 2774.90 6.944 122 2774.05 6.942 150 2772.83 6.939 192 2741.21 6.860 112 2739.87 6.856 155 2732.54 6.838 403 2724.61 6.818 288 1541.75 3.858 1000
in CDCl3
liquid film
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