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4-Chloro-2-fluoronitrobenzene

Product Name 4-Chloro-2-fluoronitrobenzene

CAS700-37-8

MFC6H3ClFNO2

MW175.54

¹³CNMR

Mass

MS-IW-3629          
4-chloro-2-fluoro-1-nitrobenzene
C6H3ClFNO2          (Mass of molecular ion:    175)

   Source Temperature: 230 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      28.0       2.8
      30.0      27.1
      31.0       4.3
      36.0       1.6
      37.0       4.0
      38.0       2.7
      46.0       1.2
      49.0       2.4
      50.0      15.9
      51.0       1.9
      56.0       2.5
      57.0       6.1
      60.0       1.3
      61.0       6.9
      62.0       5.8
      63.0      10.7
      67.0       5.2
      68.0      16.6
      69.0       5.5
      72.0       1.0
      73.0       6.5
      74.0      22.0
      75.0       8.3
      81.0       4.2
      82.0       2.8
      84.0       2.4
      85.0       2.0
      86.0       1.1
      91.0       4.5
      92.0       7.3
      93.0      39.4
      94.0      35.5
      95.0       2.5
     103.0       3.2
     105.0       1.1
     108.0       2.5
     109.0      34.9
     110.0       3.1
     111.0      11.4
     117.0      48.6
     118.0       2.8
     119.0      16.0
     128.0       4.0
     129.0      77.4
     130.0       6.4
     131.0      24.8
     132.0       1.6
     145.0      63.6
     146.0       4.2
     147.0      20.8
     148.0       1.3
     159.0       6.9
     161.0       2.4
     175.0     100.0
     176.0       6.9
     177.0      32.6
     178.0       2.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₆ H₃ Cl F N O₂	0.040 g : 0.5 ml CDCl₃
4-chloro-2-fluoro-1-nitrobenzene

    Assign.     Shift(ppm)

      A             8.065
      B             7.35
      C             7.32

     Hz     ppm     Int.

   3232.79   8.090    452
   3227.54   8.076     50
   3225.10   8.070    414
   3224.24   8.068    669
   3216.55   8.049    357
   3215.94   8.047    398
   3213.38   8.041     41
   2943.85   7.367    498
   2941.65   7.361    622
   2938.96   7.354     30
   2933.96   7.342    207
   2933.35   7.340    408
   2931.88   7.337    800
   2930.91   7.334   1000
   2929.81   7.331    615
   2928.71   7.329    247
   2927.73   7.326    426
   2925.05   7.320     37
   2922.36   7.313    547
   2921.02   7.309    539
   2920.17   7.307    423
   2918.82   7.304    400

in CDCl3

KBr disc

nujol mull

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