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p-Toluenesulfonamide

Product Name p-Toluenesulfonamide

CAS70-55-3

MFC7H9NO2S

MW171.22

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  • Mass 

    MS-NW-1770          
p-toluenesulfonamide
C7H9NO2S            (Mass of molecular ion:    171)


       Source Temperature: 200 °C
   Sample Temperature: 120 °C
   Direct, 75 eV


          27.0       1.9
      38.0       2.0
      39.0      14.3
      40.0       1.2
      41.0       3.6
      50.0       4.6
      51.0       7.0
      52.0       2.0
      53.0       1.8
      61.0       1.0
      62.0       3.7
      63.0      10.9
      64.0       3.3
      65.0      29.6
      66.0       1.9
      74.0       1.2
      75.0       1.0
      77.0       5.7
      78.0       1.5
      79.0       3.1
      89.0       8.6
      90.0       4.8
      91.0     100.0
      92.0       7.9
     106.0       6.0
     107.0      19.6
     108.0      14.0
     109.0       1.0
     139.0       1.1
     155.0      30.9
     156.0       2.7
     157.0       1.5
     171.0      38.7
     172.0       3.6
     173.0       2.0

90 MHz in DMSO-d6


  • 1H NMR 89.56 MHz
    C7 H9 N O2 S 0.043 g : 0.5 ml CDCl3
    p-toluenesulfonamide
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             7.72
      B             7.36
      C             7.26
      D             2.364
  

         Hz     ppm     Int.


        696.00   7.772    284
    689.50   7.699    174
    687.69   7.679    478
    663.19   7.405    341
    662.56   7.398    372
    654.63   7.310    283
    653.94   7.302    261
    650.25   7.261    373
    211.75   2.365   1000

DMSO-d6



KBr disc



nujol mull





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