2-MERCAPTO-4-METHYLPYRIMIDINE HYDROCHLORIDE

Mass

MS-NW-6697          
4-methyl-2-pyrimidinethiol hydrochloride
C5H6N2S HCl         (Mass of molecular ion:    126)

   Source Temperature: 160 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      15.0       3.7
      18.0       3.5
      26.0       3.3
      27.0       3.5
      28.0      10.3
      32.0       2.3
      33.0       1.7
      35.0       5.9
      36.0      44.4
      37.0       3.5
      38.0      14.1
      39.0      23.5
      40.0      10.2
      41.0      14.8
      42.0       9.9
      43.0       1.1
      44.0       2.0
      45.0       3.7
      50.0       1.3
      51.0       3.0
      52.0       6.6
      53.0       3.7
      57.0       4.2
      58.0       5.2
      59.0       8.8
      60.0       9.5
      63.0       2.1
      64.0       2.0
      65.0       1.3
      66.0      10.1
      67.0       5.9
      68.0      59.3
      69.0       3.2
      70.0       2.8
      71.0       1.0
      72.0       3.4
      81.0       1.0
      82.0       6.8
      83.0       2.0
      84.0       8.0
      85.0       3.1
      93.0       3.3
      98.0       2.2
      99.0       1.5
     111.0      26.8
     112.0       1.6
     113.0       1.3
     125.0       4.5
     126.0     100.0
     127.0       7.6
     128.0       5.1

Assign. Shift(ppm) A 9.05 B 8.534 C 7.230 D 2.426

     Hz     ppm     Int.

    810.13   9.046    430
    766.92   8.564    293
    761.94   8.508    325
    650.32   7.262    220
    649.80   7.256    211
    645.26   7.205    191
    644.75   7.200    198
    217.38   2.428   1000
    217.02   2.424    938