4-Methylpyridin-2-amine

Mass

MS-NW-1418          
4-methyl-2-pyridylamine
C6H8N2              (Mass of molecular ion:    108)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      26.0       1.0
      27.0       5.1
      28.0       8.3
      37.0       1.8
      38.0       4.2
      39.0      11.2
      40.0       3.4
      41.0       9.8
      42.0       2.7
      43.0       3.8
      50.0       2.9
      51.0       4.2
      52.0       4.5
      53.0      11.5
      54.0       3.0
      63.0       1.9
      64.0       2.1
      65.0       3.8
      66.0       6.9
      67.0       1.7
      68.0       6.4
      78.0       1.0
      79.0       1.2
      80.0      60.0
      81.0      29.6
      82.0       1.8
      91.0       1.4
      93.0       3.3
     107.0       3.2
     108.0     100.0
     109.0       7.5

Parameter ppm Hz D(A) 7.81 D(B) 6.37 D(C) 6.20 D(D) 2.16 J(A,B) 5.2 J(A,C) 0.6 J(A,D) 0.2 J(B,C) 1.5 J(B,D) 0.6 J(C,D) 0.7 D(E) 4.68 BELL,C.L. ET AL. J.HETEROCYCL.CHEM. 2, 420 (1965) J(A,D):LESS THAN 0.2HZ.

     Hz     ppm     Int.

   2345.69   7.819    160
   2340.49   7.802    164
   1914.61   6.382     73
   1913.98   6.380     87
   1913.20   6.377     91
   1909.41   6.365     73
   1908.78   6.363     86
   1907.99   6.360     88
   1860.75   6.202    160
   1860.01   6.200    177
   1859.33   6.198    154
   1403.97   4.680   1000
    648.02   2.160    903