2,2'-METHYLIMINOBIS(ACETALDEHYDE DIETHYL ACETAL)

Mass

MS-NW-5835          
N,N-bis(2,2-diethoxyethyl)methylamine
C13H29NO4           (Mass of molecular ion:    263)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       3.4
      18.0       1.8
      19.0       1.7
      26.0       1.7
      27.0       6.6
      28.0       3.8
      29.0      15.2
      30.0       1.3
      31.0      14.4
      41.0       1.9
      42.0      11.2
      43.0       6.8
      44.0      11.9
      45.0      10.5
      46.0       1.7
      47.0      33.1
      55.0       1.2
      56.0       1.4
      57.0       4.7
      58.0      14.9
      59.0      27.1
      60.0       1.5
      61.0      10.1
      70.0       3.1
      71.0       2.3
      72.0      11.0
      73.0       4.0
      74.0       1.0
      75.0      25.5
      76.0       1.0
      82.0       1.5
      84.0       2.9
      85.0       1.6
      86.0       4.9
      88.0       1.1
      89.0       5.0
      96.0       1.6
      97.0       1.2
      98.0       2.1
      99.0       1.1
     100.0       3.9
     101.0       4.1
     102.0       6.5
     103.0      30.9
     104.0       1.8
     114.0      31.7
     115.0       2.9
     116.0      28.5
     117.0       2.8
     125.0       1.2
     129.0       2.6
     130.0       2.1
     132.0       2.6
     142.0       1.1
     146.0      13.8
     147.0       3.7
     158.0       2.6
     160.0     100.0
     161.0       8.7
     171.0       1.6
     172.0      16.0
     173.0       2.3
     174.0       1.1
     204.0       3.0
     217.0       4.3
     218.0      13.0
     219.0       3.1

Assign. Shift(ppm) A 4.608 B *1 3.659 C *1 3.526 D 2.652 E 2.408 F 1.212 J(A,D)=5.2HZ. J(B,F)=J(C,F)=7.0HZ. J(B,C)=9.3HZ.

     Hz     ppm     Int.

    418.38   4.672     56
    413.13   4.613    133
    407.88   4.555     75
    339.19   3.788     48
    337.06   3.764     59
    332.06   3.708     60
    331.13   3.698     68
    329.88   3.684    181
    324.06   3.619    180
    322.75   3.604    199
    317.13   3.541    179
    315.69   3.525     84
    314.75   3.515     56
    310.19   3.464     67
    307.75   3.437     49
    240.13   2.682    208
    234.88   2.623    196
    215.63   2.408    321
    115.38   1.289    450
    108.31   1.210   1000
    101.25   1.131    386