1-METHYL-1,2,3,6-TETRAHYDROPYRIDINE

Mass

MS-NW-6409          
1-methyl-1,2,3,6-tetrahydropyridine
C6H11N              (Mass of molecular ion:     97)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       9.4
      17.0       1.1
      18.0       5.1
      26.0       2.7
      27.0      12.9
      28.0       7.2
      29.0       3.0
      30.0       3.4
      37.0       1.1
      38.0       2.3
      39.0      20.4
      40.0       2.9
      41.0      14.1
      42.0     100.0
      43.0      55.1
      44.0      19.2
      45.0       3.3
      50.0       2.3
      51.0       3.9
      52.0       4.1
      53.0       9.8
      54.0      42.1
      55.0       8.7
      56.0       2.3
      57.0       1.5
      65.0       2.0
      66.0       1.5
      67.0       6.1
      68.0      17.7
      69.0       4.6
      70.0       2.4
      78.0       1.5
      79.0       3.3
      80.0       5.9
      81.0       9.7
      82.0      23.5
      83.0       1.7
      91.0       1.2
      92.0       1.3
      93.0       1.1
      94.0      18.2
      95.0       2.5
      96.0      86.5
      97.0      92.4
      98.0       7.9

Assign. Shift(ppm) A 5.729 B 5.659 C 2.904 D 2.503 E 2.334 F 2.19

     Hz     ppm     Int.

   1166.50   2.919     89
   1163.45   2.912    211
   1161.38   2.906    221
   1160.52   2.904    241
   1158.45   2.899    213
   1155.52   2.892     89
   1006.35   2.519    220
   1000.61   2.504    412
    994.87   2.490    255
    935.79   2.342    103
    932.98   2.335   1000
    886.23   2.218     31
    883.42   2.211     62
    881.47   2.206     74
    880.62   2.204     94
    877.81   2.197    128
    875.73   2.192    119
    875.12   2.190    127
    874.27   2.188    118
    872.31   2.183    126
    869.38   2.176     88
    866.58   2.169     54