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MassMS-IW-8151 2,6-difluorobenzylamine C7H7F2N (Mass of molecular ion: 143)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
28.0 13.6 29.0 9.8 30.0 18.2 31.0 1.2 39.0 1.1 48.0 1.6 50.0 2.4 51.0 2.3 51.5 1.6 57.0 2.6 61.0 1.1 61.5 1.4 62.0 1.6 63.0 5.1 68.0 1.7 69.0 1.6 70.0 1.8 71.0 3.2 71.5 1.1 74.0 1.9 75.0 8.0 76.0 1.3 77.0 2.4 81.0 1.8 88.0 1.6 93.0 1.5 94.0 1.9 95.0 17.3 96.0 4.8 97.0 1.3 100.0 1.7 101.0 4.8 102.0 3.1 107.0 2.6 113.0 1.3 114.0 11.1 115.0 9.9 120.0 4.0 122.0 11.2 123.0 52.1 124.0 7.6 125.0 3.0 126.0 1.6 127.0 26.0 128.0 2.1 140.0 5.7 141.0 1.9 142.0 100.0 143.0 26.9 144.0 3.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H7 F2 N 0.05 ml : 0.5 ml CDCl3 2,6-difluorobenzylamine 
Assign. Shift(ppm)
A 7.170 B 6.855 C 3.895 D 1.51
Hz ppm Int.2880.86 7.209 89 2874.39 7.193 178 2872.44 7.188 148 2867.80 7.176 109 2865.97 7.172 319 2864.14 7.167 125 2859.25 7.155 149 2857.67 7.151 211 2851.07 7.134 108 2754.03 6.892 46 2752.20 6.887 62 2747.19 6.874 374 2746.22 6.872 305 2744.02 6.867 83 2740.36 6.857 330 2739.14 6.854 521 2734.25 6.842 86 2731.08 6.834 318 2725.71 6.821 50 2724.24 6.817 41 1556.27 3.895 1000 605.59 1.516 401
in CDCl3
liquid film
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