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69045-84-7More Spectrum > 2,3-Dichloro-5-(trifluoromethyl)pyridine(69045-84-7)MS
2,3-Dichloro-5-(trifluoromethyl)pyridine
Product Name 2,3-Dichloro-5-(trifluoromethyl)pyridine
CAS69045-84-7
MFC6H2Cl2F3N
MW215.99
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MS-IW-4768 2,3-dichloro-5-(trifluoromethyl)pyridine C6H2Cl2F3N (Mass of molecular ion: 215)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
28.0 1.5 31.0 2.0 37.0 1.2 49.0 2.1 50.0 3.2 51.0 2.4 60.0 1.9 62.0 1.2 67.0 3.0 68.0 1.0 69.0 18.4 74.0 1.0 75.0 9.5 76.0 4.5 80.5 1.0 84.0 3.2 85.0 5.9 86.0 1.9 87.0 2.0 91.0 1.4 93.0 1.5 94.0 2.2 95.0 1.2 98.0 1.4 99.0 2.0 107.5 1.3 109.0 2.6 110.0 4.0 111.0 1.5 112.0 1.3 119.0 2.3 126.0 1.4 130.0 3.1 132.0 1.0 133.0 1.7 144.0 2.5 146.0 1.3 153.0 4.9 155.0 1.6 160.0 14.7 161.0 1.2 162.0 5.0 165.0 2.3 167.0 1.5 180.0 65.4 181.0 5.2 182.0 20.9 183.0 1.7 196.0 9.0 197.0 1.0 198.0 6.0 215.0 100.0 216.0 7.5 217.0 64.6 218.0 4.7 219.0 10.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H2 Cl2 F3 N 0.05 ml : 0.5 ml CDCl3 2,3-dichloro-5-(trifluoromethyl)pyridine Assign. Shift(ppm)
A 8.591 B 8.034
Hz ppm Int.
3435.06 8.596 768 3434.20 8.594 843 3432.86 8.590 827 3432.01 8.588 723 3426.03 8.573 23 3425.29 8.571 20 3212.40 8.039 1000 3211.79 8.037 991 3211.06 8.035 717 3210.21 8.033 971 3209.59 8.032 904 3203.37 8.016 22 3202.88 8.015 21
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