QUINACRINE DIHYDROCHLORIDE

Mass

MS-NW-7005          
N(3)-(6-chloro-2-methoxy-9-acridinyl)-N(1),N(1)-diethyl-1,4-pentanediamine dihydrochloride
C23H30ClN3O 2HCl    (Mass of molecular ion:    399)

   Source Temperature: 210 °C
   Sample Temperature: 160 °C
   Direct, 75 eV

      15.0       1.0
      18.0       1.1
      27.0       2.8
      28.0       5.5
      29.0       6.9
      30.0      14.3
      35.0       2.9
      36.0      14.7
      37.0       1.0
      38.0       4.7
      39.0       1.8
      41.0       8.1
      42.0       6.9
      43.0       2.1
      44.0       3.7
      55.0       1.9
      56.0       7.9
      57.0       2.2
      58.0      17.7
      69.0       3.5
      70.0       3.0
      71.0       4.0
      72.0       4.6
      73.0       7.8
      74.0       1.1
      84.0       7.7
      85.0       1.5
      86.0     100.0
      87.0       6.1
      98.0       4.2
      99.0      13.0
     100.0       1.6
     112.0      15.3
     113.0       4.1
     114.0       1.1
     126.0      34.7
     127.0       3.4
     140.0       8.1
     141.0       2.0
     142.0       3.9
     164.0       2.6
     165.0       1.2
     179.0       1.6
     192.0       2.3
     199.0       1.1
     200.0       5.1
     201.0       1.4
     202.0       1.8
     214.0       1.3
     215.0       2.8
     216.0       1.1
     217.0       1.1
     228.0       1.3
     229.0       1.1
     242.0       2.1
     243.0       6.9
     244.0       6.2
     245.0       3.2
     246.0       1.9
     254.0       2.3
     255.0       1.3
     256.0       1.3
     257.0       6.5
     258.0       6.1
     259.0      15.3
     260.0       4.3
     261.0       4.6
     269.0       1.7
     270.0       1.8
     271.0       1.9
     283.0       2.5
     284.0       1.6
     285.0       5.4
     286.0       1.5
     287.0       1.6
     297.0       1.3
     298.0       1.9
     299.0       3.0
     300.0       1.1
     309.0       1.0
     311.0       3.9
     312.0       1.0
     313.0       2.2
     325.0       3.2
     326.0       4.5
     327.0       3.4
     328.0       2.2
     370.0       1.7
     399.0      14.9
     400.0       4.1
     401.0       5.3
     402.0       1.4

Assign. Shift(ppm) A 8.044 B 7.59 C 7.524 D 7.444 E 7.40 G 4.062 J 3.141 K 3.10 L 2.00 M 1.725 N 1.654 P 1.227 SOLVENT SIGNAL REMOVED

     Hz     ppm     Int.

   3219.73   8.057    114
   3210.45   8.034    123
   3036.87   7.599    155
   3034.67   7.594    221
   3033.81   7.592    253
   3033.08   7.590    272
   3008.42   7.528    151
   3006.35   7.523    198
   2980.59   7.459    105
   2978.52   7.453    109
   2971.44   7.436    102
   2969.24   7.430    106
   2960.08   7.407    108
   2958.62   7.404    119
   1623.54   4.063   1000
   1267.58   3.172    138
   1260.25   3.154    417
   1252.93   3.136    464
   1245.61   3.117    238
   1236.21   3.094    114
   1231.93   3.083     31
   1231.32   3.081     31
   1228.88   3.075     56
    692.87   1.734    382
    686.40   1.718    385
    677.49   1.696     43
    669.19   1.675     84
    661.01   1.654    108
    652.83   1.634     67
    497.80   1.246    451
    490.48   1.228    906
    483.15   1.209    450