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MassMS-NW-5469 o-methoxybenzylamine C8H11NO (Mass of molecular ion: 137)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 2.9 18.0 1.8 27.0 3.1 28.0 18.0 29.0 2.8 30.0 38.9 37.0 1.3 38.0 3.5 39.0 11.6 40.0 2.0 41.0 3.6 42.0 1.5 50.0 6.1 51.0 14.9 52.0 5.3 53.0 2.1 54.0 1.8 55.0 1.0 61.0 1.0 62.0 2.2 63.0 6.5 64.0 3.5 65.0 15.6 66.0 8.4 67.0 3.8 74.0 1.9 75.0 1.8 76.0 3.2 77.0 25.4 78.0 16.7 79.0 11.0 80.0 1.3 89.0 3.4 90.0 4.1 91.0 41.1 92.0 7.7 93.0 10.9 94.0 10.3 95.0 7.9 102.0 1.7 103.0 1.3 104.0 24.7 105.0 12.1 106.0 49.2 107.0 16.1 108.0 15.9 109.0 11.7 110.0 1.0 119.0 13.2 120.0 29.1 121.0 43.3 122.0 17.3 123.0 1.5 133.0 1.3 134.0 4.4 136.0 100.0 137.0 73.6 138.0 6.9
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H11 N O 0.04 ml : 0.5 ml CDCl3 o-methoxybenzylamine 
Assign. Shift(ppm)
A 7.22 B 7.19 C 6.90 D 6.86 E 3.826 F 3.81 G 1.54
Hz ppm Int.653.81 7.301 26 649.81 7.256 55 647.88 7.235 93 646.25 7.216 43 643.31 7.184 44 641.25 7.161 93 640.75 7.155 79 639.81 7.144 95 625.31 6.983 48 623.94 6.967 79 617.94 6.900 114 616.63 6.886 101 610.63 6.819 35 609.31 6.804 65 607.81 6.787 32 344.44 3.846 27 342.69 3.827 1000 340.88 3.807 394 138.19 1.543 615
in CDCl3
liquid film
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