5,N-DIMETHYL-3-(4-FLUOROPHENYL)-4-ISOXAZOLECARBOXAMIDE)
Product Name 5,N-DIMETHYL-3-(4-FLUOROPHENYL)-4-ISOXAZOLECARBOXAMIDE)
CAS67764-99-2
MFC12H11FN2O2
MW234.23
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MassMS-IW-0832 3-(p-fluorophenyl)-N,5-dimethyl-4-isoxazolecarboxamide C12H11FN2O2 (Mass of molecular ion: 234)
Source Temperature: 130 °C Sample Temperature: 110 °C Direct, 75 eV
15.0 1.3 28.0 1.2 30.0 1.6 43.0 38.4 44.0 1.2 57.0 1.5 58.0 4.3 75.0 4.1 82.0 4.5 84.0 1.0 94.0 1.8 95.0 8.4 96.0 2.0 97.0 1.4 107.0 4.8 108.0 1.8 109.0 11.2 110.0 1.2 111.0 4.7 112.0 1.1 117.0 1.1 121.0 3.6 122.0 2.9 123.0 3.5 124.0 8.7 125.0 13.4 126.0 1.0 133.0 1.4 134.0 11.8 135.0 6.6 136.0 1.6 146.0 1.2 147.0 2.7 148.0 8.1 149.0 1.6 160.0 1.5 161.0 5.8 162.0 88.9 163.0 14.0 164.0 4.2 175.0 1.3 176.0 1.1 177.0 5.4 191.0 4.8 192.0 5.1 204.0 4.6 205.0 2.0 206.0 1.0 216.0 1.2 217.0 1.1 219.0 10.4 220.0 1.4 233.0 6.9 234.0 100.0 235.0 14.8 236.0 1.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H11 F N2 O2 0.037 g : 0.5 ml CDCl3 3-(p-fluorophenyl)-N,5-dimethyl-4-isoxazolecarboxamide 
Assign. Shift(ppm)
A 7.601 B 7.185 C 5.60 D 2.811 E 2.658
Hz ppm Int.3045.04 7.620 127 3042.97 7.615 67 3039.79 7.607 143 3038.33 7.603 91 3037.72 7.601 91 3036.25 7.598 155 3033.20 7.590 74 3031.01 7.585 142 2879.88 7.207 139 2877.81 7.201 57 2873.05 7.189 73 2871.34 7.185 235 2869.38 7.180 73 2864.75 7.169 55 2862.55 7.163 126 2239.14 5.603 30 1126.22 2.819 521 1121.34 2.806 526 1062.26 2.658 1000
in CDCl3
KBr disc
nujol mull
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