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67367-37-7

PYRAZINE-2,3-DICARBOXYLIC ACID MONOAMIDE

Product Name PYRAZINE-2,3-DICARBOXYLIC ACID MONOAMIDE

CAS67367-37-7

MFC6H5N3O3

MW167.12

More

  • 67367-37-7_ms_1
    Mass

    MS-IW-4870          
    3-carbamoyl-2-pyrazinecarboxylic acid
    C6H5N3O3            (Mass of molecular ion:    167)
    

       Source Temperature: 170 °C
       Sample Temperature: 160 °C
       Direct, 75 eV
    

          16.0       1.6
          17.0       1.7
          18.0       3.0
          25.0       1.1
          26.0      19.3
          27.0       1.8
          28.0      19.7
          29.0       1.0
          38.0       2.1
          39.0       2.8
          40.0       2.7
          41.0       2.5
          42.0       1.4
          43.0       1.6
          44.0      48.9
          45.0       5.3
          50.0       2.0
          51.0      16.6
          52.0      54.3
          53.0      56.8
          54.0       3.4
          67.0       1.6
          68.0       3.6
          69.0       1.7
          70.0       3.6
          77.0       3.7
          78.0      29.4
          79.0      28.7
          80.0     100.0
          81.0       5.6
          95.0       1.0
          96.0       1.4
          97.0       1.4
         105.0       5.2
         106.0      20.0
         107.0       2.6
         123.0      96.4
         124.0      13.2
         149.0      11.5
         150.0       3.7
         168.0       1.2
    

400 MHz in DMSO-d6

  • 67367-37-7_1hnmr_0

    1H NMR 399.65 MHz
    C6 H5 N3 O3 0.038 g : 0.5 ml DMSO-d6
    3-carbamoyl-2-pyrazinecarboxylic acid
    ChemicalStructure
        Assign.     Shift(ppm)
    A 13.6 B *1 8.849 C *1 8.812 D *2 8.30 E *2 7.92

         Hz     ppm     Int.
    

       5450.01  13.637     62
       3543.31   8.867     23
       3538.18   8.854    762
       3535.62   8.847    994
       3530.49   8.834     24
       3529.85   8.833     22
       3527.71   8.828     31
       3523.01   8.816   1000
       3520.66   8.810    701
       3319.37   8.306    214
       3166.58   7.924    213
    

in DMSO-d6

  • 67367-37-7_13cnmr_0

KBr disc

  • 67367-37-7_ir1_2

nujol mull

  • 67367-37-7_ir2_1