SpectrumDetail Supplier Related Products
WebSite > CAS DataBase List  > 6651-36-1More Spectrum  >1-Cyclohexenyloxytrimethylsilane(6651-36-1)IR1

1-Cyclohexenyloxytrimethylsilane

CAS6651-36-1

MFC9H18OSi

MW170.32

More


  • Mass

    MS-IW-7536          
    1-(trimethylsilyloxy)cyclohexene
    C9H18OSi            (Mass of molecular ion:    170)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0       2.9
          28.0       1.0
          29.0       1.2
          39.0       3.3
          41.0       5.4
          42.0       2.4
          43.0       5.2
          44.0       2.9
          45.0      15.5
          46.0       1.0
          47.0       5.5
          51.0       1.2
          53.0       2.9
          55.0       5.9
          56.0       1.6
          57.0       2.4
          58.0       1.3
          59.0       7.4
          60.0       1.1
          61.0       4.4
          63.5       1.1
          66.0       1.1
          67.0       1.0
          68.0       1.5
          69.0       1.9
          70.0       5.1
          71.0       1.2
          72.0       2.3
          73.0      75.5
          74.0       6.7
          75.0     100.0
          76.0       9.4
          77.0       7.8
          77.5       1.4
          78.0       1.3
          79.0       5.6
          80.0       2.2
          81.0       3.1
          83.0       1.0
          85.0       7.1
          97.0       1.1
          98.0       2.5
          99.0       3.7
         101.0       1.3
         111.0       1.8
         113.0       1.9
         125.0       1.0
         127.0      53.0
         128.0       6.4
         129.0       2.8
         141.0       6.5
         142.0      26.1
         143.0       3.7
         144.0       1.1
         147.0       7.3
         148.0       1.1
         151.0       1.4
         155.0      69.5
         156.0       9.8
         157.0       3.2
         169.0      40.0
         170.0      74.2
         171.0      12.6
         172.0       3.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9 H18 O Si 0.05 ml : 0.5 ml CDCl3
    1-(trimethylsilyloxy)cyclohexene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.860 B 1.99 C *1 1.651 D *1 1.509 E 0.174

         Hz     ppm     Int.
    

       1942.50   4.861     45
        802.49   2.008     51
        800.66   2.004     53
        799.80   2.002     56
        798.58   1.999     49
        796.26   1.993     59
        794.43   1.988     65
        793.09   1.985     60
        666.50   1.668     35
        660.89   1.654     37
        654.79   1.639     35
        607.42   1.520     37
        604.98   1.514     31
        601.93   1.507     43
        595.95   1.492     38
         73.12   0.183     70
         69.58   0.175   1000
         66.53   0.167     87
         64.82   0.163     45
    

in CDCl3



liquid film