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MS-NW-9889 o-nitrobenzaldehyde oxime C7H6N2O3 (Mass of molecular ion: 166)
Source Temperature: 190 °C Sample Temperature: 190 °C Direct, 75 eV
17.0 2.2 18.0 12.1 27.0 3.7 28.0 6.2 29.0 1.3 30.0 7.7 37.0 1.9 38.0 3.7 39.0 22.6 40.0 1.4 41.0 2.9 44.0 1.4 50.0 18.6 51.0 22.8 52.0 11.8 53.0 4.4 61.0 1.2 62.0 4.1 63.0 14.1 64.0 15.4 65.0 36.0 66.0 3.5 74.0 4.8 75.0 12.6 76.0 25.7 77.0 16.0 78.0 21.1 79.0 19.5 80.0 2.5 88.0 1.8 89.0 4.3 90.0 10.0 91.0 25.0 92.0 12.0 93.0 3.9 102.0 18.9 103.0 7.8 104.0 6.7 105.0 6.6 107.0 1.3 118.0 2.5 119.0 4.7 132.0 2.7 134.0 5.0 135.0 100.0 136.0 16.2 137.0 1.4 148.0 3.0 149.0 4.1 166.0 15.3 167.0 3.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H6 N2 O3 0.031 g : 0.5 ml CDCl3 o-nitrobenzaldehyde oxime Assign. Shift(ppm)
A 8.70 B 8.697 C 8.079 D 7.902 E 7.666 F 7.574
Hz ppm Int.
3475.95 8.698 1000 3233.15 8.090 441 3232.18 8.088 414 3231.81 8.087 430 3224.98 8.070 484 3223.63 8.067 464 3163.57 7.916 366 3162.11 7.913 377 3155.76 7.897 438 3154.30 7.893 436 3072.51 7.689 181 3072.02 7.687 205 3071.29 7.685 209 3070.68 7.684 197 3068.12 7.678 38 3064.58 7.669 399 3063.84 7.667 376 3063.35 7.666 387 3057.37 7.651 222 3056.76 7.649 252 3056.03 7.647 234 3055.42 7.646 223 3034.67 7.594 318 3033.20 7.590 319 3027.22 7.575 295 3026.49 7.573 369 3026.00 7.572 336 3025.15 7.570 345 3021.48 7.561 44 3019.04 7.555 210 3017.58 7.551 197
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