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65753-47-1

2-Chloro-3-(trifluoromethyl)pyridine

Product Name 2-Chloro-3-(trifluoromethyl)pyridine

CAS65753-47-1

MFC6H3ClF3N

MW181.54

More

  • 65753-47-1_ms_1
    Mass

    MS-IW-2145          
    2-chloro-3-(trifluoromethyl)pyridine
    C6H3ClF3N           (Mass of molecular ion:    181)
    

       Source Temperature: 230 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          26.0       2.1
          28.0       1.0
          31.0       2.8
          37.0       1.5
          38.0       1.9
          39.0       1.6
          49.0       2.2
          50.0       8.2
          51.0       6.6
          52.0       1.4
          57.0       1.5
          62.0       1.1
          69.0      18.0
          70.0       1.4
          74.0       1.0
          75.0       9.1
          76.0       9.0
          77.0       2.1
          81.0       1.1
          84.0       1.0
          85.0       3.1
          87.0       1.3
          93.0       2.0
          95.0       1.0
          96.0       4.5
          99.0       3.2
         100.0       2.3
         112.0       1.8
         119.0       4.6
         120.0       1.9
         126.0      27.9
         127.0       2.7
         146.0     100.0
         147.0       7.1
         162.0       8.6
         164.0       2.9
         181.0      95.7
         182.0       6.7
         183.0      30.9
         184.0       2.2
    

400 MHz in CDCl3

  • 65753-47-1_1hnmr

    1H NMR 399.65 MHz
    C6 H3 Cl F3 N 0.056 g : 0.5 ml CDCl3
    2-chloro-3-(trifluoromethyl)pyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.592 B 8.046 C 7.407

         Hz     ppm     Int.
    

       3436.52   8.599    812
       3435.18   8.596    873
       3431.76   8.587    885
       3430.42   8.584    898
       3220.46   8.059    893
       3219.85   8.057    877
       3218.51   8.054    943
       3212.65   8.039    965
       3212.16   8.038    951
       3210.82   8.035   1000
       2967.04   7.425    764
       2966.31   7.423    764
       2962.16   7.412    794
       2961.43   7.411    787
       2959.23   7.405    797
       2958.50   7.403    773
       2954.35   7.393    739
       2953.74   7.391    719
    

in CDCl3

  • 65753-47-1_13cnmr_0

KBr disc

  • 65753-47-1_ir1_2

nujol mull

  • 65753-47-1_ir2_1