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MassMS-NW-9909 N(1)-(5-methoxy-2-pyrimidinyl)sulfanilamide C11H12N4O3S (Mass of molecular ion: 280)
Source Temperature: 230 °C Sample Temperature: 160 °C Direct, 75 eV
15.0 1.3 18.0 4.2 27.0 1.2 28.0 6.1 39.0 6.6 41.0 2.1 42.0 1.5 52.0 1.8 53.0 2.0 54.0 6.2 55.0 1.2 63.0 2.3 64.0 3.5 65.0 34.7 66.0 4.2 70.0 2.4 80.0 1.7 82.0 5.9 83.0 1.0 91.0 3.4 92.0 53.4 93.0 5.4 97.0 1.5 108.0 27.1 109.0 3.2 110.0 12.2 111.0 1.2 118.0 1.1 119.0 3.5 124.0 1.1 125.0 16.4 126.0 1.7 140.0 2.8 146.0 2.2 156.0 9.0 157.0 1.1 172.0 2.5 173.0 6.5 174.0 1.6 200.0 2.8 201.0 12.2 202.0 1.5 215.0 100.0 216.0 93.6 217.0 12.0 281.0 1.4
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C11 H12 N4 O3 S 0.037 g : 0.5 ml DMSO-d6 N(1)-(5-methoxy-2-pyrimidinyl)sulfanilamide 
Assign. Shift(ppm)
A 11.0 B 8.283 C 7.615 D 6.580 E 6.00 F 3.436
Hz ppm Int.4411.56 11.039 38 3310.55 8.284 1000 3050.64 7.634 30 3048.07 7.627 271 3046.24 7.623 78 3041.11 7.610 84 3039.28 7.605 290 3036.53 7.598 35 2636.86 6.598 35 2634.12 6.592 290 2632.29 6.587 83 2627.34 6.575 85 2625.33 6.570 287 2622.58 6.563 35 2396.37 5.997 226 1373.38 3.437 1000
in DMSO-d6
KBr disc
nujol mull
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