400 MHz in CDCl3
90 MHz in CDCl3
-
1H NMR 399.65 MHz C12 H28 Si 0.05 ml : 0.5 ml CDCl3 triisobutylsilane 
Assign. Shift(ppm)
A 4.685 B 1.838 C 0.963 D *1 0.660 E *1 0.581 J(SI-29,H(A))=200.1HZ J(D,E)=-14.9HZ 90MHZ : HSP-06-060
Hz ppm Int.1877.44 4.698 30 1875.37 4.693 66 1874.51 4.691 69 1872.44 4.686 110 1870.36 4.680 75 1869.51 4.678 66 1867.43 4.673 33 748.17 1.873 57 741.46 1.856 101 734.86 1.839 116 734.13 1.837 113 727.54 1.821 105 720.95 1.804 63 401.49 1.005 46 398.32 0.997 70 388.18 0.972 1000 381.47 0.955 978 371.70 0.931 56 369.38 0.925 49 278.69 0.698 57 275.63 0.690 60 271.97 0.681 58 269.04 0.674 59 263.79 0.661 123 260.86 0.653 126 257.20 0.644 120 254.27 0.637 118 241.70 0.605 137 239.62 0.600 139 234.25 0.587 129 232.18 0.581 134 226.93 0.568 67 224.85 0.563 66 219.48 0.550 63 217.41 0.545 62
-
1H NMR 89.56 MHz C12 H28 Si 0.04 ml : 0.5 ml CDCl3 triisobutylsilane Assign. Shift(ppm)
A 4.678 B 1.81 C 0.964 D *1 0.66 E *1 0.60 400MHZ : HSP-43-045
Hz ppm Int.421.56 4.708 41 419.00 4.679 60 416.56 4.652 41 172.13 1.922 33 165.44 1.848 43 159.06 1.777 38 158.25 1.767 38 89.31 0.998 1000 82.94 0.927 789 61.13 0.683 98 59.63 0.666 110 58.38 0.652 113 57.31 0.640 112 54.56 0.610 92 52.06 0.582 132 50.00 0.559 87
in CDCl3
liquid film
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