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MassMS-IW-1022 homatropine hydrochloride C16H21NO3 HCl (Mass of molecular ion: 275)
Source Temperature: 190 °C Sample Temperature: 150 °C Direct, 75 eV
30.0 1.1 36.0 9.0 38.0 3.2 39.0 1.6 41.0 3.1 42.0 8.1 44.0 2.2 51.0 2.3 53.0 1.0 55.0 3.1 56.0 1.6 57.0 2.2 65.0 1.2 67.0 10.9 68.0 3.0 70.0 1.8 77.0 9.0 78.0 1.6 79.0 7.0 80.0 1.8 81.0 2.8 82.0 25.9 83.0 18.0 84.0 1.9 90.0 1.1 91.0 2.5 93.0 2.2 94.0 15.8 95.0 8.5 96.0 12.4 97.0 3.1 105.0 5.9 106.0 4.1 107.0 6.6 108.0 1.7 118.0 1.1 122.0 1.7 123.0 4.3 124.0 100.0 125.0 11.9 140.0 5.9 142.0 12.1 143.0 1.1 275.0 21.4 276.0 4.1
400 MHz in D2O
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1H NMR 399.65 MHz C16 H21 N O3 saturated in D2O homatropine hydrochloride 
Assign. Shift(ppm)
A 7.49 B 5.380 C 5.080 D *1 3.83 E *1 3.651 F 2.679 G *2 2.363 J *2 2.271 K *3 2.15 to 2.18 L 1.86 M *3 1.122 SOLVENT PEAK REMOVED
Hz ppm Int.2992.92 7.489 732 2150.15 5.381 381 2030.52 5.081 97 1529.79 3.828 57 1463.01 3.661 54 1459.35 3.652 49 1455.57 3.643 55 1070.68 2.680 1000 953.98 2.388 39 953.61 2.387 39 941.41 2.356 36 937.38 2.346 54 916.50 2.294 39 900.02 2.253 47 866.21 2.168 65 864.14 2.163 45 850.34 2.128 65 849.85 2.127 65 843.63 2.111 48 842.29 2.108 53 841.92 2.107 54 841.43 2.106 52 838.50 2.099 63 838.01 2.097 63 837.65 2.096 63 837.28 2.096 63 836.79 2.094 63 832.64 2.084 101 827.03 2.070 63 826.42 2.068 62 752.69 1.884 61 751.22 1.880 73 750.61 1.879 74 750.00 1.877 70 748.54 1.873 59 747.56 1.871 56 735.96 1.842 58 734.62 1.839 69 734.13 1.837 69 445.07 1.114 53
in D2O
KBr disc
nujol mull
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