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MS-IW-7531 tetraphenylethylene C26H20 (Mass of molecular ion: 332)
Source Temperature: 150 °C Sample Temperature: 130 °C Direct, 75 eV
51.0 1.1 77.0 1.2 113.0 1.2 119.5 1.2 125.0 1.0 126.0 3.9 126.5 1.4 127.0 3.4 138.0 1.9 143.5 1.4 144.5 2.6 145.0 2.1 150.0 3.1 150.5 1.6 151.0 4.2 151.5 1.3 152.0 2.8 156.5 2.5 157.0 2.0 157.5 1.3 158.0 1.6 163.0 1.6 165.0 4.5 166.0 3.3 167.0 2.9 176.0 1.7 177.0 1.6 178.0 3.5 215.0 1.3 226.0 1.4 228.0 1.1 239.0 5.7 240.0 3.6 241.0 7.1 242.0 1.5 250.0 2.1 251.0 1.0 252.0 11.7 253.0 17.5 254.0 13.1 255.0 13.0 256.0 2.5 265.0 1.0 276.0 1.1 289.0 2.6 290.0 1.1 291.0 2.6 302.0 2.1 303.0 1.7 313.0 1.1 315.0 3.0 316.0 1.8 317.0 3.3 326.0 1.0 327.0 1.0 329.0 1.5 330.0 1.5 331.0 4.4 332.0 100.0 333.0 28.5 334.0 4.0 366.0 1.8
90 MHz in CDCl3
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1H NMR 89.56 MHz C26 H20 0.032 g : 0.5 ml CDCl3 tetraphenylethylene Assign. Shift(ppm)
A 7.06
Hz ppm Int.
640.00 7.147 32 639.00 7.135 36 636.06 7.103 78 634.06 7.080 279 632.31 7.061 1000 629.19 7.026 218 625.25 6.982 64 624.25 6.971 59 623.56 6.963 65 620.81 6.932 30 620.25 6.926 28 619.19 6.914 24
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