AMYL-2-METHYLVALERATE

Mass

MS-IW-3577          
pentyl 2-methylvalerate
C11H22O2            (Mass of molecular ion:    186)

   Source Temperature: 220 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      27.0      15.8
      28.0       5.9
      29.0      24.0
      31.0       2.3
      39.0       9.4
      40.0       2.0
      41.0      34.8
      42.0      28.1
      43.0      90.1
      44.0       4.5
      45.0       3.7
      53.0       2.1
      55.0      28.7
      56.0       7.3
      57.0       4.7
      59.0       1.8
      67.0       1.0
      69.0       9.6
      70.0      63.5
      71.0      86.7
      72.0       5.3
      73.0       4.7
      74.0      71.0
      75.0       9.6
      85.0       1.1
      87.0      16.9
      88.0       1.3
      89.0       1.9
      99.0      55.5
     100.0       4.1
     101.0       3.0
     115.0       7.0
     116.0       3.3
     117.0     100.0
     118.0       7.1
     144.0      11.9
     145.0       1.0
     157.0       1.3

Assign. Shift(ppm) A *1 4.07 B *1 4.06 C 2.439 D 1.67 to 1.60 E 1.40 F 1.38 to 1.30 G 1.139 J 0.91

     Hz     ppm     Int.

   1631.47   4.083    204
   1630.49   4.080    199
   1624.76   4.066    402
   1623.90   4.064    377
   1617.92   4.049    207
   1617.19   4.047    203
    985.47   2.466     66
    978.27   2.448    107
    971.56   2.432    109
    964.72   2.414     75
    675.90   1.692     34
    669.43   1.676     57
    668.21   1.672     45
    666.26   1.668     61
    662.96   1.659     85
    661.74   1.656     92
    660.64   1.654    103
    658.81   1.649    140
    655.27   1.640    186
    652.83   1.634    152
    651.86   1.632    185
    649.29   1.625    125
    647.83   1.621    193
    644.65   1.614    130
    642.58   1.608     73
    641.24   1.605     67
    640.50   1.603     71
    637.82   1.596     55
    572.51   1.433     41
    566.16   1.417     82
    563.35   1.410     64
    559.81   1.401     66
    557.01   1.394    151
    553.96   1.387     58
    550.66   1.378    128
    549.44   1.375    124
    544.31   1.362    225
    542.24   1.357    405
    538.09   1.347    432
    534.91   1.339    492
    533.20   1.335    210
    530.76   1.329    385
    527.71   1.321    198
    526.25   1.317    120
    523.68   1.311    203
    521.36   1.305     97
    520.51   1.303     86
    517.94   1.296     53
    516.48   1.293     95
    514.40   1.288     75
    509.28   1.275     30
    507.57   1.271     33
    458.86   1.149   1000
    456.42   1.143     75
    451.90   1.131    952
    374.63   0.938     66
    370.97   0.929    315
    369.63   0.925    564
    367.55   0.920    214
    366.21   0.917    239
    364.01   0.911    695
    362.43   0.907    890
    356.81   0.893    262
    355.10   0.889    391
    349.61   0.875     45