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MassMS-NW-2646 n-methyltrimethylenediamine C4H12N2 (Mass of molecular ion: 88)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 3.0 17.0 1.1 18.0 7.5 27.0 2.2 28.0 12.9 29.0 2.7 30.0 38.6 31.0 6.8 32.0 3.6 39.0 1.1 41.0 3.6 42.0 11.8 43.0 7.5 44.0 100.0 45.0 7.4 56.0 15.0 57.0 17.9 58.0 10.4 70.0 8.6 71.0 42.8 72.0 2.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C4 H12 N2 0.05 ml : 0.5 ml CDCl3 N-methyltrimethylenediamine 
Assign. Shift(ppm)
A 2.77 B 2.64 C 2.43 D 1.63 E 1.36
Hz ppm Int.254.63 2.844 125 247.75 2.767 267 243.31 2.717 181 241.13 2.693 209 236.56 2.642 271 229.69 2.565 179 224.50 2.507 39 217.25 2.426 1000 160.06 1.788 88 159.19 1.778 95 152.81 1.707 384 145.94 1.630 483 139.31 1.556 223 138.75 1.550 226 134.38 1.501 25 132.56 1.481 69 131.69 1.471 67 129.50 1.446 28 121.94 1.362 734
in CDCl3
liquid film
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