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MS-NW-4685 1-chloroheptane C7H15Cl (Mass of molecular ion: 134)
Source Temperature: 260 °C Sample Temperature: 170 °C Reservoir, 75 eV
15.0 1.2 26.0 1.7 27.0 24.3 28.0 2.9 29.0 33.0 36.0 1.3 39.0 16.3 40.0 3.1 41.0 70.5 42.0 23.7 43.0 73.4 44.0 2.5 49.0 2.9 51.0 1.3 53.0 3.6 54.0 3.5 55.0 57.2 56.0 43.2 57.0 31.0 58.0 1.5 63.0 5.2 65.0 1.7 67.0 1.7 68.0 2.8 69.0 46.0 70.0 20.4 71.0 4.6 77.0 1.2 83.0 2.8 85.0 1.0 91.0 100.0 92.0 5.0 93.0 31.8 94.0 1.7 98.0 1.2 105.0 7.5 107.0 2.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H15 Cl 0.04 ml : 0.5 ml CDCl3 1-chloroheptane Assign. Shift(ppm)
A 0.89 B 1.18 to 1.56 C 1.77 D 3.52
Hz ppm Int.
322.25 3.599 383 320.63 3.581 46 320.44 3.578 46 315.69 3.525 1000 313.75 3.504 58 309.00 3.451 590 307.63 3.435 41 307.25 3.431 35 165.13 1.844 91 158.19 1.767 161 152.13 1.699 134 139.63 1.560 51 118.06 1.319 919 85.00 0.950 207 79.56 0.889 781 73.50 0.821 151
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