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MassMS-NW-5611 1-methylbutylamine C5H13N (Mass of molecular ion: 87)
Source Temperature: 280 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.6 18.0 7.2 27.0 3.5 28.0 2.7 29.0 1.6 30.0 11.0 39.0 2.3 41.0 3.5 42.0 5.3 43.0 2.9 44.0 100.0 45.0 2.6 55.0 2.2 56.0 1.0 72.0 5.2 86.0 1.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C5 H13 N 0.04 ml : 0.5 ml CDCl3 1-methylbutylamine 
Assign. Shift(ppm)
A 2.879 B 1.36 to 1.24 C 1.26 D 1.053 E 0.92
Hz ppm Int.261.81 2.924 46 255.56 2.854 49 126.38 1.412 41 124.63 1.392 33 122.94 1.373 96 122.19 1.365 136 120.06 1.341 127 118.63 1.325 205 117.13 1.308 107 116.44 1.301 116 115.38 1.289 189 114.56 1.280 108 113.31 1.266 1000 110.63 1.236 61 97.38 1.088 844 95.44 1.066 41 91.06 1.017 783 89.38 0.998 62 88.06 0.984 88 87.56 0.978 97 84.88 0.948 80 84.19 0.941 87 82.06 0.917 219 78.25 0.874 46 76.94 0.860 47 75.81 0.847 74 74.69 0.834 46 74.06 0.827 33
in CDCl3
liquid film
4880 A,200 M,liquid
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