3-[(p-nitrophenyl)hydrazono]butan-2-one oxime

Mass

MS-NW-6908          
biacetyl mono(p-nitrophenylhydrazone) monooxime
C10H12N4O3          (Mass of molecular ion:    236)

   Source Temperature: 230 °C
   Sample Temperature: 170 °C
   Direct, 75 eV

      15.0      15.4
      17.0       2.4
      18.0       9.7
      26.0       1.8
      27.0       7.9
      28.0       9.5
      29.0       1.6
      30.0      74.7
      31.0       4.9
      37.0       1.6
      38.0       6.4
      39.0      13.3
      40.0       6.4
      41.0      14.9
      42.0      44.8
      43.0       8.4
      44.0       3.0
      50.0       8.1
      51.0       6.6
      52.0      11.2
      53.0       7.7
      54.0       4.0
      55.0       2.5
      57.0       1.4
      58.0      11.6
      61.0       1.0
      62.0       5.0
      63.0      26.1
      64.0      25.7
      65.0       9.9
      66.0       1.9
      67.0       1.4
      68.0       8.0
      69.0       6.8
      70.0       4.7
      74.0       2.3
      75.0       8.3
      76.0      10.7
      77.0       4.3
      78.0       4.6
      79.0      10.3
      80.0       9.2
      81.0       3.6
      82.0       1.0
      83.0       4.1
      84.0       3.2
      88.0       1.0
      89.0       5.2
      90.0      31.5
      91.0      22.4
      92.0      10.5
      93.0       2.1
      98.0       1.1
      99.0       2.1
     100.0       1.4
     102.0       1.3
     103.0       1.8
     104.0       2.8
     105.0       6.7
     106.0      17.2
     107.0       4.8
     108.0       8.9
     109.0       1.0
     116.0       1.0
     117.0       1.9
     118.0       1.5
     119.0       1.3
     120.0       3.2
     121.0       1.7
     122.0      23.1
     123.0       2.2
     130.0       1.2
     131.0       5.6
     132.0       6.7
     133.0       1.5
     135.0       1.0
     136.0      25.1
     137.0       8.9
     138.0      15.6
     139.0       3.1
     143.0       1.1
     144.0       1.5
     145.0       1.7
     146.0       1.1
     147.0       3.0
     150.0       9.8
     151.0      14.5
     152.0       3.2
     156.0       1.5
     157.0       1.0
     158.0       1.2
     161.0       2.7
     162.0       1.3
     163.0       1.2
     172.0       4.3
     173.0      25.2
     174.0       3.6
     177.0       8.4
     178.0       2.7
     188.0      12.9
     189.0       3.2
     190.0       1.4
     202.0       5.3
     203.0       2.4
     204.0       2.3
     206.0       1.3
     218.0      17.6
     219.0      77.3
     220.0      14.6
     221.0       2.2
     234.0       4.2
     235.0       2.5
     236.0     100.0
     237.0      15.3
     238.0       2.3

Assign. Shift(ppm) A *1 11.4 B *1 10.2 C 8.143 D 7.324 E *2 2.153 F *2 2.082

     Hz     ppm     Int.

   4577.14  11.453    184
   4095.24  10.248    153
   3259.45   8.156    272
   3250.11   8.133    280
   2934.69   7.344     34
   2931.76   7.336    233
   2927.18   7.325     22
   2922.42   7.313    223
   2919.49   7.306     31
    860.52   2.154    940
    832.13   2.083   1000