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MS-NW-5811 ethyl N-ethylcarbamate C5H11NO2 (Mass of molecular ion: 117)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 5.8 18.0 4.7 19.0 1.0 26.0 3.1 27.0 22.8 28.0 10.8 29.0 80.7 30.0 100.0 31.0 7.9 40.0 1.2 41.0 1.8 42.0 5.1 43.0 4.4 44.0 29.7 45.0 11.6 46.0 2.6 56.0 6.3 58.0 8.5 62.0 2.4 71.0 3.5 72.0 35.9 73.0 3.2 74.0 10.9 88.0 28.0 89.0 10.6 90.0 1.3 102.0 41.1 103.0 2.2 117.0 10.6
90 MHz in CDCl3
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1H NMR 89.56 MHz C5 H11 N O2 0.04 ml : 0.5 ml CDCl3 ethyl N-ethylcarbamate Assign. Shift(ppm)
A 4.83 B 4.108 C 3.200 D 1.237 E 1.133
Hz ppm Int.
378.94 4.232 120 371.75 4.151 384 364.63 4.072 404 357.63 3.994 139 301.13 3.363 47 293.75 3.280 151 287.94 3.216 143 286.56 3.200 165 280.75 3.135 151 279.63 3.123 72 273.63 3.056 58 117.88 1.317 469 114.13 1.275 33 110.81 1.238 958 108.63 1.213 500 103.69 1.158 433 101.50 1.134 1000 98.31 1.098 41 95.88 1.071 30 94.19 1.052 397
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