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MassMS-KW-0552 2,2,3-tribromobutane C4H7Br3 (Mass of molecular ion: 292)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
26.0 3.9 27.0 27.2 28.0 3.0 29.0 10.2 37.0 1.2 38.0 2.3 39.0 11.8 43.0 1.1 49.0 1.0 50.0 4.3 51.0 6.5 52.0 2.4 53.0 58.2 54.0 5.8 55.0 35.0 56.0 1.8 79.0 3.3 80.0 5.3 81.0 3.3 82.0 5.2 93.0 1.0 105.0 3.3 107.0 9.8 109.0 6.4 119.0 1.1 133.0 26.4 134.0 8.3 135.0 26.3 136.0 7.6 137.0 1.0 185.0 2.9 187.0 5.7 189.0 2.7 213.0 51.6 214.0 3.4 215.0 100.0 216.0 4.9 217.0 48.4 218.0 2.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C4H7Br3 0.05 ml : 0.5 ml CDCl3 2,2,3-tribromobutane 
Assign. Shift(ppm)
A 4.453 B 2.668 C 2.040
Hz ppm Int.1789.80 4.477 72 1783.33 4.461 205 1776.74 4.445 208 1770.27 4.429 76 1066.53 2.668 1000 1066.29 2.668 993 818.73 2.048 666 812.26 2.032 655
in CDCl3
Liquid film
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