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MS-IW-7199 tripropyl orthoformate C10H22O3 (Mass of molecular ion: 190)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
18.0 2.4 26.0 1.6 27.0 14.7 28.0 5.0 29.0 5.0 31.0 28.7 37.0 1.6 38.0 2.4 39.0 14.4 40.0 5.4 41.0 37.8 42.0 31.6 43.0 97.1 44.0 6.3 45.0 1.2 47.0 21.8 57.0 1.4 58.0 1.0 59.0 5.3 60.0 2.1 63.0 2.8 73.0 1.0 88.0 1.3 89.0 100.0 90.0 5.0 105.0 1.5 131.0 83.3 132.0 6.6 189.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H22 O3 0.05 ml : 0.5 ml CDCl3 tripropyl orthoformate Assign. Shift(ppm)
A 5.154 B 3.503 C 1.625 D 0.949
Hz ppm Int.
2059.81 5.155 329 1406.86 3.521 448 1400.02 3.504 756 1393.31 3.487 452 667.97 1.672 66 660.64 1.654 210 653.69 1.636 395 646.36 1.618 395 639.53 1.601 239 632.20 1.582 77 386.47 0.968 649 379.03 0.949 1000 371.58 0.930 582
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