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4-(Dimethylamino)cinnamaldehyde

Product Name 4-(Dimethylamino)cinnamaldehyde

CAS6203-18-5

MFC11H13NO

MW175.23

¹³CNMR

Mass

MS-NW-1691          
p-(dimethylamino)cinnamaldehyde
C11H13NO            (Mass of molecular ion:    175)

   Source Temperature: 250 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       3.2
      17.0       2.5
      18.0      10.8
      27.0       2.8
      28.0       3.2
      29.0       3.6
      30.0       1.3
      38.0       1.4
      39.0       5.7
      41.0       1.6
      42.0       8.6
      43.0       1.1
      44.0       4.3
      50.0       5.2
      51.0      11.0
      52.0       2.7
      53.0       1.4
      55.0       1.8
      60.5       2.4
      62.0       2.2
      63.0       7.0
      64.0       2.5
      64.5       2.2
      65.0       3.7
      66.0       1.9
      69.0       1.4
      72.5       7.6
      73.0       2.6
      73.5       8.1
      74.0       3.0
      75.0       4.6
      76.0       4.0
      77.0      16.7
      78.0       4.0
      79.0       2.5
      86.5       3.0
      87.0       1.8
      89.0       3.9
      90.0       2.1
      91.0       4.7
      92.0       1.0
     101.0       3.8
     102.0       7.9
     103.0      13.2
     104.0       5.6
     105.0       4.1
     106.0       1.4
     115.0       2.3
     116.0       2.5
     117.0       2.5
     118.0       2.9
     119.0       2.5
     120.0      18.5
     121.0      47.2
     122.0       4.2
     128.0       2.5
     129.0       2.7
     130.0      10.8
     131.0      18.2
     132.0       8.2
     133.0       1.2
     134.0      11.8
     135.0       1.3
     144.0       6.7
     145.0       4.1
     146.0      34.1
     147.0      17.9
     148.0       2.5
     158.0       3.6
     159.0       1.4
     160.0       1.5
     161.0       1.2
     174.0      37.6
     175.0     100.0
     176.0      12.4

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₁ H₁₃ N O	0.041 g : 0.5 ml CDCl₃
p-(dimethylamino)cinnamaldehyde

    Assign.     Shift(ppm)

      A             9.581
      B             7.40
      C             7.32
      D             6.67
      E             6.53
      F             3.013
     
     J(A,E)=7.6HZ. J(C,E)=15.7HZ.

     Hz     ppm     Int.

    861.99   9.625     97
    854.37   9.540    102
    668.92   7.469     63
    668.48   7.465     72
    666.72   7.445     23
    666.36   7.441     24
    665.04   7.426     37
    661.89   7.391     25
    661.60   7.388     24
    659.84   7.368     96
    659.33   7.362     78
    649.00   7.247     62
    601.54   6.717     88
    599.41   6.693     26
    593.77   6.630     71
    592.53   6.617     69
    586.16   6.545     57
    578.10   6.455     40
    570.48   6.370     36
    269.82   3.013   1000

in CDCl3

KBr disc

nujol mull

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