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M-TOLUAMIDE

Product Name M-TOLUAMIDE

CAS618-47-3

MFC8H9NO

MW135.16

¹³CNMR

Mass

MS-NW-9024          
m-toluamide
C8H9NO              (Mass of molecular ion:    135)

   Source Temperature: 260 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      38.0       1.0
      39.0       6.0
      41.0       1.3
      44.0       2.9
      50.0       2.2
      51.0       3.5
      52.0       1.0
      62.0       2.4
      63.0       6.4
      64.0       1.8
      65.0      17.7
      66.0       1.1
      77.0       1.8
      89.0       7.0
      90.0       5.1
      91.0      77.0
      92.0       6.5
     106.0       1.0
     116.0       2.6
     117.0       3.7
     118.0       1.4
     119.0     100.0
     120.0       9.0
     135.0      62.9
     136.0       6.2

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₈ H₉ N O	0.036 g : 0.5 ml CDCl₃
m-toluamide

    Assign.     Shift(ppm)

      A             7.66
      B             7.65
      C             7.35
      D             7.34
      E             6.6
      F             2.357
     
     CONFIRMED BY LAOCN PROGRAM

     Hz     ppm     Int.

    685.19   7.651    239
    683.88   7.637    188
    680.69   7.601    113
    679.50   7.588     79
    677.25   7.562     86
    676.69   7.556     83
    675.50   7.543     62
    658.38   7.352     80
    656.00   7.325    363
    655.13   7.315    254
    649.81   7.256    131
    590.94   6.599     50
    211.19   2.359   1000

in CDCl3

KBr disc

nujol mull

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