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1-Methyl-1-phenylhydrazine

Product Name 1-Methyl-1-phenylhydrazine

CAS618-40-6

MFC7H10N2

MW122.17

¹³CNMR

Mass

MS-KW-0242          
1-methyl-1-phenylhydrazine
C7H10N2             (Mass of molecular ion:    122)

   Source Temperature: 240 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       1.8
      16.0       1.0
      17.0       1.1
      18.0       1.9
      27.0       3.3
      28.0       5.1
      29.0       9.6
      30.0       2.2
      37.0       1.4
      38.0       3.2
      39.0       9.8
      40.0       1.0
      41.0       1.0
      42.0       1.1
      43.0       4.9
      45.0       1.8
      50.0       8.2
      51.0      23.9
      52.0       7.3
      52.5       1.1
      53.0       4.1
      53.5       1.7
      61.0       3.9
      62.0       1.4
      63.0       5.2
      64.0       3.7
      65.0       8.3
      66.0       2.8
      74.0       2.7
      75.0       2.0
      76.0       2.2
      77.0      90.2
      78.0      17.3
      79.0      21.9
      80.0       2.5
      90.0       1.0
      91.0       4.3
      92.0       6.9
      93.0       7.6
      94.0       2.0
     104.0      11.6
     105.0      10.7
     106.0      25.0
     107.0      68.5
     108.0       5.4
     121.0       8.6
     122.0     100.0
     123.0       8.7
     133.0       3.4
     134.0       3.9

400 MHz in CDCl3

90 MHz in CDCl3

¹H NMR	399.65 MHz
C₇H₁₀N₂	0.05 ml : 0.5 ml CDCl₃
1-methyl-1-phenylhydrazine

    Assign.     Shift(ppm)

     A           7.208
     B           6.924
     C           6.765
     D           3.56
     E           2.983

     Hz     ppm     Int.

   2892.09   7.235     40
   2889.90   7.229    213
   2888.92   7.227     99
   2887.70   7.224     87
   2884.89   7.217     53
   2882.57   7.211    264
   2881.72   7.209    180
   2880.99   7.207    274
   2878.79   7.201     55
   2875.86   7.194     94
   2874.52   7.191    102
   2873.66   7.189    249
   2871.46   7.183     44
   2774.42   6.940     61
   2772.34   6.935    264
   2771.25   6.932    310
   2770.39   6.930    180
   2769.05   6.927    105
   2765.51   6.918     93
   2764.53   6.916    152
   2763.43   6.913    260
   2762.46   6.910    235
   2760.01   6.904     42
   2712.41   6.785     68
   2711.31   6.782    116
   2710.33   6.780     70
   2705.08   6.767    112
   2704.11   6.764    195
   2703.01   6.762    111
   2697.76   6.749     57
   2696.78   6.746     99
   2695.68   6.743     60
   1421.03   3.555    153
   1192.27   2.983   1000

¹H NMR	89.56 MHz
C₇ H₁₀ N₂	0.04 ml : 0.5 ml CDCl₃
1-methyl-1-phenylhydrazine

    Assign.     Shift(ppm)

      A             7.23
      B             6.98
      C             6.80
      D             3.59
      E             3.061

     Hz     ppm     Int.

    657.69   7.344     31
    656.94   7.336     38
    650.50   7.264     64
    649.25   7.250     65
    648.75   7.244     72
    648.13   7.237     85
    643.81   7.189     65
    642.25   7.172     57
    641.81   7.167     88
    641.13   7.159     91
    628.75   7.021     96
    627.31   7.005    134
    624.94   6.978     32
    621.13   6.936     30
    619.88   6.922     67
    618.50   6.906     58
    615.81   6.876     41
    614.63   6.863     40
    607.50   6.784     59
    600.50   6.706     31
    321.13   3.586     92
    274.13   3.061   1000

in CDCl3

KBr disc

liquid film

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