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MS-NW-8674 1,2,4-tribromobenzene C6H3Br3 (Mass of molecular ion: 312)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
37.0 4.8 38.0 2.6 49.0 3.5 50.0 5.8 61.0 1.0 73.0 7.0 74.0 30.0 75.0 29.4 76.0 2.1 76.5 1.7 77.0 5.9 77.5 2.1 78.0 5.5 79.0 1.3 80.0 1.0 81.0 1.2 82.0 1.0 116.0 2.9 116.5 1.2 117.0 5.4 117.5 2.3 118.0 2.9 118.5 1.2 128.0 2.4 130.0 2.4 153.0 7.5 154.0 13.4 155.0 8.5 156.0 14.4 157.0 7.5 158.0 6.4 159.0 2.1 233.0 19.2 234.0 2.3 235.0 37.7 236.0 3.8 237.0 18.4 238.0 1.7 312.0 34.4 313.0 2.3 314.0 100.0 315.0 6.7 316.0 97.1 317.0 6.4 318.0 31.5 319.0 2.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H3 Br3 0.021 g : 0.5 ml CDCl3 1,2,4-tribromobenzene Assign. Shift(ppm)
A 7.773 B 7.471 C 7.290
Hz ppm Int.
3107.42 7.776 887 3104.98 7.770 946 2990.97 7.484 788 2982.42 7.463 1000 2920.41 7.308 727 2918.21 7.302 582 2915.04 7.294 24 2911.87 7.287 543 2909.67 7.281 536 2907.84 7.276 23
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