2,2 DIMETHYL-4-CYANOBUTYRALDEHYDE

Mass

MS-IW-3500          
4,4-dimethyl-5-oxovaleronitrile
C7H11NO             (Mass of molecular ion:    125)

   Source Temperature: 220 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      15.0       1.5
      26.0       2.3
      27.0      19.0
      28.0       7.6
      29.0      21.0
      30.0       1.6
      31.0       3.5
      37.0       1.2
      38.0       2.7
      39.0      23.4
      40.0       4.2
      41.0      78.1
      42.0      33.5
      43.0      21.1
      50.0       2.0
      51.0       4.2
      52.0       4.3
      53.0      12.9
      54.0      17.8
      55.0     100.0
      56.0      10.7
      57.0      36.4
      58.0       1.7
      59.0       1.3
      65.0       1.2
      66.0       1.3
      67.0       3.5
      68.0      15.4
      69.0      73.8
      70.0       5.0
      71.0       3.5
      72.0       1.8
      79.0       5.1
      80.0       2.5
      81.0       3.1
      82.0       7.5
      83.0       1.5
      85.0       1.2
      94.0       1.6
      96.0      91.7
      97.0      22.1
      98.0       2.5

Assign. Shift(ppm) A 9.446 B 2.330 C 1.896 D 1.129

     Hz     ppm     Int.

   3775.02   9.446    348
    939.82   2.352    147
    935.67   2.342     34
    932.86   2.335    122
    932.13   2.333    177
    930.79   2.330    111
    927.86   2.322     38
    923.95   2.312    171
    765.75   1.917    165
    761.84   1.907     30
    759.03   1.900     94
    757.57   1.896    159
    754.15   1.888     35
    749.76   1.877    136
    451.42   1.130   1000