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MassMS-NW-7597 N-ethyl-N-methylaniline C9H13N (Mass of molecular ion: 135)
Source Temperature: 240 °C Sample Temperature: 170 °C Reservoir, 75 eV
15.0 1.2 18.0 1.2 27.0 2.5 28.0 1.7 29.0 1.2 39.0 3.4 42.0 4.9 44.0 1.3 50.0 2.2 51.0 7.9 52.0 1.9 60.0 3.3 63.0 1.8 64.0 1.1 65.0 2.5 66.0 1.0 67.5 1.3 77.0 19.1 78.0 3.4 79.0 3.9 91.0 4.1 92.0 1.9 93.0 1.4 103.0 2.2 104.0 9.4 105.0 10.1 106.0 8.1 117.0 1.1 118.0 3.5 119.0 2.6 120.0 100.0 121.0 10.7 132.0 1.8 133.0 1.1 134.0 6.7 135.0 33.1 136.0 3.6
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H13 N 0.05 ml : 0.5 ml CDCl3 N-ethyl-N-methylaniline 
Assign. Shift(ppm)
A 7.19 B 6.70 C 6.67 D 3.356 E 2.858 F 1.084 B AND C WERE CONFIRMED BY LAOCN PROGRAM.
Hz ppm Int.653.94 7.302 67 653.38 7.296 70 651.25 7.272 38 647.56 7.231 71 646.81 7.223 97 645.56 7.209 122 644.44 7.196 171 642.56 7.175 44 640.63 7.154 58 637.94 7.124 141 637.50 7.119 150 635.88 7.101 59 635.25 7.094 37 605.75 6.764 56 603.38 6.738 302 600.69 6.708 75 596.38 6.660 224 595.13 6.646 145 594.19 6.635 132 591.06 6.600 36 590.19 6.590 47 589.06 6.578 54 588.00 6.566 30 311.38 3.477 64 304.25 3.398 196 297.19 3.319 209 290.19 3.241 77 259.44 2.897 56 256.06 2.860 1000 104.19 1.164 287 101.69 1.136 34 101.25 1.131 36 97.19 1.086 586 93.75 1.047 34 90.06 1.006 250
in CDCl3
liquid film
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