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MassMS-NW-4851 acetophenone oxime C8H9NO (Mass of molecular ion: 135)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 3.8 17.0 1.1 18.0 5.2 27.0 3.4 28.0 1.9 37.0 1.3 38.0 2.4 39.0 6.3 40.0 1.5 41.0 1.3 42.0 7.9 43.0 8.3 50.0 10.8 51.0 31.0 52.0 4.4 59.0 1.1 62.0 1.4 63.0 3.1 64.0 1.0 65.0 5.5 66.0 8.2 74.0 2.9 75.0 2.7 76.0 7.5 77.0 100.0 78.0 24.4 79.0 3.0 89.0 1.8 90.0 1.4 91.0 4.6 92.0 2.9 93.0 1.9 94.0 15.3 95.0 1.1 102.0 1.8 103.0 15.9 104.0 17.2 105.0 62.5 106.0 10.8 107.0 3.7 117.0 1.8 118.0 8.4 119.0 9.1 120.0 16.9 121.0 1.6 134.0 6.3 135.0 40.0 136.0 3.8
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H9 N O 0.02 ml : 0.5 ml CDCl3 acetophenone oxime 
Assign. Shift(ppm)
A 2.299 B 2.599 C 7. D 7.27 to 8.03
Hz ppm Int.717.44 8.011 45 715.88 7.994 42 707.69 7.902 56 687.88 7.681 53 684.50 7.643 56 683.94 7.637 44 682.31 7.619 56 680.75 7.602 69 679.38 7.586 59 677.94 7.570 103 674.13 7.528 56 672.31 7.507 92 666.88 7.447 44 666.13 7.438 50 664.75 7.423 93 663.88 7.413 48 662.81 7.401 136 661.56 7.387 71 660.38 7.374 74 659.38 7.363 136 658.31 7.351 66 657.81 7.345 61 656.13 7.327 146 232.75 2.599 621 205.88 2.299 1000
in CDCl3
CCl4 solution
KBr disc
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