ALPHA,ALPHA,ALPHA-TRIBROMOQUINALDINE
Product Name ALPHA,ALPHA,ALPHA-TRIBROMOQUINALDINE
CAS613-53-6
MFC10H6Br3N
MW379.87
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MassMS-IW-0689 2-(tribromomethyl)quinoline C10H6Br3N (Mass of molecular ion: 377)
Source Temperature: 160 °C Sample Temperature: 120 °C Direct, 75 eV
39.0 1.6 50.0 1.4 51.0 1.2 56.0 1.0 56.5 1.1 62.0 1.4 63.0 3.7 69.5 1.6 70.0 5.2 70.5 1.5 74.0 1.0 75.0 1.5 79.0 1.4 80.0 5.2 81.0 1.4 82.0 5.2 87.0 1.4 88.0 1.6 89.0 1.1 101.0 1.1 109.5 5.6 110.0 1.2 110.5 5.5 111.0 1.1 113.0 7.0 114.0 2.8 139.0 2.3 140.0 43.3 141.0 7.1 149.0 3.7 150.0 7.3 151.0 3.6 193.0 1.7 195.0 1.6 218.0 1.7 219.0 5.4 220.0 8.2 221.0 5.9 222.0 6.4 298.0 51.2 299.0 6.5 300.0 100.0 301.0 12.5 302.0 49.4 303.0 6.1 377.0 1.6 379.0 4.7 381.0 4.6 383.0 1.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H6 Br3 N 0.038 g : 0.5 ml CDCl3 2-(tribromomethyl)quinoline 
Assign. Shift(ppm)
A 8.250 B 8.242 C 8.203 D 7.863 E 7.791 F 7.606
Hz ppm Int.3305.54 8.272 64 3296.51 8.249 690 3294.80 8.245 1000 3286.01 8.223 111 3283.08 8.215 218 3282.47 8.214 225 3274.54 8.194 246 3273.93 8.192 250 3147.58 7.876 168 3147.09 7.875 180 3146.24 7.873 188 3138.92 7.855 214 3138.06 7.853 227 3122.31 7.813 142 3120.85 7.809 133 3115.36 7.796 187 3113.89 7.792 272 3112.43 7.788 130 3106.93 7.775 168 3105.47 7.771 145 3055.91 7.647 179 3054.69 7.644 175 3048.95 7.630 166 3047.73 7.626 285 3046.63 7.624 158 3040.77 7.609 128 3039.67 7.606 121
in CDCl3
KBr disc
nujol mull
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