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MS-NW-1268 4-benzylbiphenyl C19H16 (Mass of molecular ion: 244)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
39.0 2.0 51.0 2.1 63.0 1.8 65.0 2.1 77.0 1.7 78.0 1.1 89.0 1.5 91.0 8.1 115.0 4.8 122.0 1.3 128.0 1.2 139.0 1.3 141.0 1.6 151.0 1.0 152.0 5.1 153.0 3.1 164.0 1.2 165.0 18.9 166.0 9.4 167.0 16.8 168.0 2.3 202.0 1.6 203.0 1.0 215.0 2.8 216.0 1.1 226.0 1.0 227.0 1.2 228.0 4.4 229.0 5.5 230.0 1.0 239.0 2.2 240.0 1.0 241.0 3.3 242.0 1.8 243.0 18.6 244.0 100.0 245.0 20.4 246.0 2.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C19 H16 11.6 mg : 0.5 ml CDCl3 4-benzylbiphenyl Assign. Shift(ppm)
A 7.564 B 7.512 C 7.413 D 7.32 E 7.30 F 7.26 G 7.22 J 7.21 K 4.021
Hz ppm Int.
3028.81 7.579 381 3027.47 7.576 470 3025.51 7.571 156 3022.22 7.563 162 3021.36 7.561 228 3020.39 7.558 546 3019.65 7.556 404 3019.17 7.555 528 3017.21 7.550 113 3015.50 7.546 49 3014.16 7.543 42 3013.79 7.542 41 3011.84 7.537 41 3008.91 7.529 83 3006.84 7.524 550 3004.88 7.519 231 3000.49 7.508 222 2998.41 7.503 694 2996.46 7.498 143 2994.02 7.492 46 2993.04 7.490 42 2991.33 7.485 32 2972.78 7.439 78 2971.80 7.437 193 2971.07 7.435 303 2969.24 7.430 132 2967.53 7.426 43 2966.67 7.424 40 2965.70 7.421 106 2965.09 7.420 132 2963.75 7.416 572 2962.40 7.413 274 2959.23 7.405 50 2957.52 7.401 172 2955.93 7.397 328 2955.44 7.396 298 2953.86 7.392 85 2950.44 7.383 32 2940.80 7.359 34 2932.86 7.339 144 2931.64 7.336 262 2930.30 7.333 167 2928.96 7.329 45 2927.25 7.325 141 2926.27 7.323 288 2924.19 7.317 329 2922.12 7.312 132 2919.80 7.306 319 2918.58 7.303 401 2917.97 7.302 376 2916.87 7.299 255 2915.65 7.296 143 2913.57 7.291 169 2911.62 7.286 436 2910.89 7.284 344 2909.79 7.281 158 2906.98 7.274 123 2904.91 7.269 597 2904.42 7.268 507 2902.95 7.264 233 2900.88 7.259 82 2898.44 7.253 198 2897.09 7.250 428 2896.48 7.248 550 2893.68 7.241 289 2891.60 7.236 1000 2889.77 7.231 368 2887.82 7.226 152 2886.84 7.224 181 2886.35 7.223 191 2885.62 7.221 261 2885.01 7.219 344 2884.40 7.218 339 2883.67 7.216 374 2881.59 7.211 269 2879.39 7.205 97 2878.17 7.202 67 2875.85 7.196 82 2874.51 7.193 103 2873.54 7.191 57 2873.05 7.189 61 1606.93 4.021 866 1599.12 4.002 30
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