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MS-NW-9573 1,3,5-triphenylbenzene C24H18 (Mass of molecular ion: 306)
Source Temperature: 200 °C Sample Temperature: 150 °C Direct, 75 eV
138.0 1.2 144.5 1.3 151.0 1.2 153.0 2.4 202.0 2.1 203.0 1.2 215.0 1.5 226.0 4.1 227.0 2.5 228.0 5.1 229.0 3.0 276.0 1.8 277.0 1.1 289.0 6.9 290.0 3.7 291.0 2.8 302.0 3.6 303.0 3.5 304.0 2.8 305.0 2.9 306.0 100.0 307.0 26.4 308.0 3.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C24 H18 0.040 g : 0.5 ml CDCl3 1,3,5-triphenylbenzene Assign. Shift(ppm)
A 7.774 B 7.681 C 7.460 D 7.371
Hz ppm Int.
3107.18 7.775 1000 3075.93 7.697 335 3074.58 7.694 421 3072.51 7.689 129 3068.48 7.678 233 3067.50 7.676 440 3066.89 7.674 356 3066.28 7.673 383 3064.33 7.668 68 2990.23 7.483 82 2989.26 7.480 169 2988.53 7.478 240 2986.69 7.474 104 2981.20 7.460 476 2979.98 7.457 250 2974.98 7.444 144 2973.51 7.441 283 2971.44 7.436 61 2952.76 7.389 114 2951.42 7.386 205 2950.20 7.382 121 2946.04 7.372 91 2943.97 7.367 229 2942.02 7.362 71 2937.99 7.352 59 2936.65 7.349 94 2935.42 7.345 52
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