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Triphenylphosphine

Product Name Triphenylphosphine

CAS603-35-0

MFC18H15P

MW262.29

¹³CNMR

Mass

MS-NW-1445          
triphenylphosphine
C18H15P             (Mass of molecular ion:    262)

   Source Temperature: 260 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      18.0       2.5
      39.0       2.4
      50.0       1.3
      51.0       5.3
      57.0       2.5
      63.0       1.3
      65.0       1.4
      77.0       2.2
      81.0       1.8
      83.0       1.0
     107.0      11.3
     108.0      33.2
     109.0       2.8
     115.0       2.6
     128.0       1.0
     131.0       1.7
     133.0       2.3
     139.0       1.0
     141.0       1.2
     152.0       5.9
     153.0       1.4
     154.0       1.6
     157.0       2.6
     170.0       2.1
     183.0      50.5
     184.0      11.9
     185.0       9.8
     186.0       1.3
     261.0      13.5
     262.0     100.0
     263.0      19.8
     264.0       1.8
     294.0       1.2

parameter in benzene-d6

90 MHz in CDCl3

¹H NMR	300 MHz
C₁₈ H₁₅ P	12 wt% in benzene-d₆
triphenylphosphine

    Parameter     ppm  Hz

      D(A)         7.236
      D(B)         6.934
      D(C)         6.926
       J(A,A')         1.707
       J(A,B)          7.632
       J(A,B')         0.607
       J(A,C)          1.240
       J(A,X)          7.518
       J(A',B)         0.607
       J(A',B')        7.632
       J(A',C)         1.240
       J(A',X)         7.518
       J(B,B')         1.391
       J(B,C)          7.442
       J(B,X)          1.435
       J(B',C)         7.442
       J(B',X)         1.435
       J(C,X)          0.747
     
     RADICS,L. ET AL. ORG.MAGN.RESON. 6, 60 (1974)

     Hz     ppm     Int.

   2183.99   7.280     25
   2182.30   7.274     29
   2180.44   7.268    104
   2179.46   7.265    279
   2178.26   7.261    158
   2177.30   7.258    183
   2175.78   7.253    367
   2174.81   7.249    266
   2172.23   7.241    598
   2170.00   7.233    545
   2168.55   7.228    234
   2166.37   7.221    275
   2165.12   7.217    305
   2163.16   7.211    270
   2162.43   7.208    317
   2160.03   7.200     34
   2159.13   7.197     48
   2093.07   6.977     23
   2091.75   6.972     25
   2091.22   6.971     25
   2089.11   6.964     63
   2087.55   6.958    174
   2086.47   6.955    180
   2085.62   6.952    156
   2083.23   6.944    686
   2082.23   6.941    818
   2081.18   6.937    614
   2079.36   6.931   1000
   2077.58   6.925    579
   2076.73   6.922    939
   2075.59   6.919    634
   2073.87   6.913    386
   2071.71   6.906    148
   2068.60   6.895     48
   2065.57   6.885     15

¹H NMR	89.56 MHz
C₁₈ H₁₅ P	0.046 g : 0.5 ml CDCl₃
triphenylphosphine

    Assign.     Shift(ppm)

      A          7.88 to 7.08

     Hz     ppm     Int.

    661.25   7.384     30
    660.63   7.377     32
    657.25   7.339   1000
    653.56   7.298    899

in CDCl3

CCl4 solution

KBr disc

nujol mull

4880 A,200 M,powder

RED. OF MOO2(CYS-OET)2, 77K

RED. OF MOO2(CYS-OET)2, RT

VO(II)CL3 COMPLEX, POWDER, RT

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