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MS-NW-9688 o-chlorobenzyl bromide C7H6BrCl (Mass of molecular ion: 204)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
39.0 1.9 44.0 2.1 44.5 1.6 50.0 1.0 51.0 1.1 62.0 2.4 63.0 4.9 73.0 1.2 84.0 2.4 85.0 2.6 89.0 13.0 90.0 3.7 91.0 1.8 99.0 4.0 101.0 1.3 125.0 100.0 126.0 8.6 127.0 32.9 128.0 2.7 160.0 1.6 162.0 1.0 204.0 7.1 206.0 9.2 208.0 2.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H6 Br Cl 0.05 ml : 0.5 ml CDCl3 o-chlorobenzyl bromide Assign. Shift(ppm)
A 7.364 B 7.324 C 7.19 D 7.18 E 4.534
Hz ppm Int.
2948.36 7.378 178 2945.19 7.370 123 2944.34 7.368 152 2942.50 7.363 214 2939.09 7.355 221 2936.28 7.348 43 2935.18 7.345 36 2934.69 7.344 39 2932.37 7.338 174 2928.96 7.329 173 2927.12 7.325 148 2925.78 7.321 111 2922.97 7.314 230 2919.31 7.305 44 2880.25 7.207 76 2879.64 7.206 62 2875.98 7.197 487 2872.80 7.189 302 2872.07 7.187 286 2870.36 7.183 287 2869.75 7.181 261 2866.58 7.173 459 2862.92 7.164 46 2862.18 7.162 53 1812.26 4.535 1000
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